• 专利标题:   Preparing oleic acid-lanthanum trifluoride-graphene composite lubricating oil anti-wear agent comprises e.g. adding ammonium fluoride and graphene oxide to solution of ethanol, and adding lanthanum nitrate solution dropwise.
  • 专利号:   CN106978232-A, CN106978232-B
  • 发明人:   KANG W, LIU J, DING L, LIAN J, ZHANG Z
  • 专利权人:   SICHUAN CARBON WORLD TECHNOLOGY CO LTD
  • 国际专利分类:   C10M141/02, C10M169/04, C10M177/00, C10N030/06, C10N030/10
  • 专利详细信息:   CN106978232-A 25 Jul 2017 C10M-141/02 201761 Pages: 6 Chinese
  • 申请详细信息:   CN106978232-A CN10263087 21 Apr 2017
  • 优先权号:   CN10263087

▎ 摘  要

NOVELTY - Preparing oleic acid-lanthanum trifluoride-graphene composite lubricating oil anti-wear agent comprises: adding ammonium fluoride and graphene oxide to aqueous solution of ethanol, adding lanthanum nitrate solution dropwise at 60-100 degrees C for 2.5-3.5 hours; adding 120-200 ml of a saturated ethanol solution containing 2-5ml oleic acid; after 3 hours, until the product gradually cooled to room temperature after filtration, washing with deionized water and ethanol repeatedly, and finally drying at 80-100 degrees C for 12-20 hours to produce the anti-wear agent. USE - The anti-wear agent is useful for producing lubricating oil. ADVANTAGE - The process produces lubricating oil anti-wear agent that has good thermal stability and chemical stability, can prevent oxidation and react with metal in a thermal environment, provides lubricating oil with more excellent stability, lubricating property, performance, wear-resistant anti-friction performance, and can be widely used in car and other rails and other mechanical friction and wear field. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are also included for: (1) the lubricating oil anti-wear agent prepared by the method; and (2) preparing a lubricating oil by using a lubricating oil anti-wear agent prepared by the method, comprising adding the prepared lubricating oil anti-wear agent to the base oil at a different mass ratio, where the base oil comprises 0.01-2% dispersant and 0.01-1% emulsifier, the milling time is 10-30 minutes, then carrying out the ultrasonic dispersion for 10-30 minutes, and then stirring the mixture thoroughly to obtain the lubricating oil.