• 专利标题:   Preparation of amorphous nano-porous titanium dioxide-supported graphene photocatalytic thin film involves forming graphene oxide coating layer on surface of amorphous nano-porous titanium dioxide strip by Czochralski method.
  • 专利号:   CN104815638-A
  • 发明人:   LIU E, LI F, WANG H, YU F, YUAN G, JIN X
  • 专利权人:   UNIV TAIYUAN TECHNOLOGY
  • 国际专利分类:   B01J021/18, B01J035/10
  • 专利详细信息:   CN104815638-A 05 Aug 2015 B01J-021/18 201619 Pages: 9 Chinese
  • 申请详细信息:   CN104815638-A CN10228118 07 May 2015
  • 优先权号:   CN10228118

▎ 摘  要

NOVELTY - Preparation of amorphous nano-porous titanium dioxide-supported graphene photocatalytic thin film involves forming a nano-porous thin film structure with uniform pore distribution and then oxidizing graphite through strong oxidizing agent and obtaining a graphene oxide solution, and then forming graphene oxide coating layer on surface of the amorphous nano-porous titanium dioxide strip by Czochralski method, and then carrying out oxidation/reduction reaction. USE - Preparation of amorphous nano-porous titanium dioxide-supported graphene photocatalytic thin film (claimed). ADVANTAGE - The method efficiently and economically provides amorphous nano-porous titanium dioxide-supported graphene photocatalytic thin film under low reaction conditions. DETAILED DESCRIPTION - Preparation of amorphous nano-porous titanium dioxide-supported graphene photocatalytic thin film involves applying constant-voltage to amorphous alloy strip in an electrochemical three-electrode system with 25-55% nitric acid solution as an electrolyte solution, using electrochemical workstation and carrying out constant-voltage electrochemical corrosion at45-85 degrees C for 3600-10800 seconds and voltage of 0.5-1.5V, and forming a nano-porous thin film structure with uniform pore distribution and then oxidizing graphite through strong oxidizing agent and obtaining a graphene oxide solution, and then forming graphene oxide coating layer on surface of the amorphous nano-porous titanium dioxide strip by Czochralski method, and then carrying out oxidation/reduction reaction.