• 专利标题:   Preparing composite piezoelectric material based on electrostatic spinning useful in flexible sensor, and underwater sound, comprises e.g. adding ethanol, deionized water and potassium hydroxide, performing ultrasonic oscillation, and preparing solvent for electrospinning.
  • 专利号:   CN115045044-A
  • 发明人:   FANG J
  • 专利权人:   SUZHOU JIEBING SENSING TECHNOLOGY CO LTD
  • 国际专利分类:   D01D005/00, D01F001/10, D01F006/48, D04H001/4318, D04H001/728
  • 专利详细信息:   CN115045044-A 13 Sep 2022 D04H-001/728 202292 Chinese
  • 申请详细信息:   CN115045044-A CN10765448 30 Jun 2022
  • 优先权号:   CN10765448

▎ 摘  要

NOVELTY - Preparing composite piezoelectric material based on electrostatic spinning comprises (i) adding 10 ml ethanol, 190 ml deionized water and 0.2 g potassium hydroxide to beaker, adjusting pH of the solution to 10 using aqueous ammonia, stirring, adding 2 g barium titanate particles, performing ultrasonic oscillation, mechanical stirring for each 1 hour, centrifuging, drying at 120℃ to obtain methacryloxypropyl trimethoxy silane-modified boron titanate particle particles, (ii) preparing solvent for electrospinning, where solvent is dimethylformamide-acetone system, stirring and mixing 6 g dimethylformamide and 4 g acetone to obtain the solvent for spinning, (iii) mixing 1 g polyvinylidene fluoride powder, 0.05-0.20 g methacryloxypropyl trimethoxy silane-modified boron titanate, mixing graphene oxide with 10 g electrostatic spinning solvent, (iv) limiting parameter of electrostatic spinning device, and (v) preparing composite piezoelectric material fiber film. USE - The method is useful for preparing composite piezoelectric material based on electrostatic spinning, which is useful in flexible sensor, underwater sound, electro-acoustic, and medical treatment. ADVANTAGE - The composite piezoelectric material has flexibility of organic polymer material, strong electric property of inorganic ceramic. The method is simple, economical, easy to prepare into any shape and large area film, suitable for mass production; uses lead-free barium titanate; and avoids lead pollution.