• 专利标题:   Preparation of silver-reduced graphene oxide-bismuth vanadate composite photocatalyst by dissolving bismuth(III) nitrate pentahydrate into nitric acid solution, stirring, and dissolving ammonium metavanadate into sodium hydroxide solution.
  • 专利号:   CN105597754-A
  • 发明人:   CHEN T, DU M, FAN Z, XU X, ZHANG Q, ZHAO D, CHU X, WU T, XIONG S
  • 专利权人:   UNIV CHONGQING TECHNOLOGY BUSINESS
  • 国际专利分类:   B01J023/68
  • 专利详细信息:   CN105597754-A 25 May 2016 B01J-023/68 201651 Pages: 9 Chinese
  • 申请详细信息:   CN105597754-A CN10117776 02 Mar 2016
  • 优先权号:   CN10117776

▎ 摘  要

NOVELTY - A silver-reduced graphene oxide-bismuth vanadate composite photocatalyst is prepared by dissolving bismuth(III) nitrate pentahydrate into nitric acid solution, uniformly stirring to obtain solution A, dissolving ammonium metavanadate into sodium hydroxide solution, uniformly stirring to obtain solution B, ultrasonically dispersing graphene oxide with water to obtain solution C, dissolving silver nitrate into ethanediol to obtain solution D, uniformly mixing solutions A and B, regulating pH value, adding solutions C and D, uniformly mixing, and hydrothermal reacting. USE - Method for preparing silver-reduced graphene oxide-bismuth vanadate composite photocatalyst (claimed). ADVANTAGE - The product has silver-bismuth vanadate micron level spherical of 5-8 mu m, increases quantum use efficiency, enhances catalytic activity, and facilitates electron transfer. DETAILED DESCRIPTION - A silver-reduced graphene oxide-bismuth vanadate composite photocatalyst is prepared by dissolving bismuth(III) nitrate pentahydrate into nitric acid solution, uniformly stirring to obtain solution A, dissolving ammonium metavanadate into sodium hydroxide solution, uniformly stirring to obtain solution B, ultrasonically dispersing graphene oxide with water to obtain solution C, dissolving silver nitrate into ethanediol to obtain solution D, uniformly mixing solutions A and B, regulating pH value to 7.0, adding solutions C and D, uniformly mixing, ultrasonically processing, transferring into hydrothermal reaction kettle for hydrothermal reaction, cooling to room temperature, collecting, generating precipitate, washing, and drying. The ratio of bismuth(III) nitrate pentahydrate and ammonium metavanadate is 1:1.