• 专利标题:   Producing composite composition of zinc oxide and graphene oxide, comprises e.g. mixing zinc chloride and graphene oxide obtained by mixing e.g. sodium nitrate and sulfuric acid, and treating with water and sodium hydroxide solution.
  • 专利号:   KR1798776-B1
  • 发明人:   JO H H, CHOI H K, JEON M H
  • 专利权人:   UNIV INJE IND ACADEMIC COOP FOUND
  • 国际专利分类:   A01N059/00, B01J006/00, C01B031/04, C01G009/02
  • 专利详细信息:   KR1798776-B1 16 Nov 2017 C01G-009/02 201780 Pages: 7
  • 申请详细信息:   KR1798776-B1 KR088805 13 Jul 2016
  • 优先权号:   KR088805

▎ 摘  要

NOVELTY - Producing composite composition, comprises (a) mixing 100 pts. wt. sodium nitrate, 430-460 pts. wt. sulfuric acid and 580-600 pts. wt. potassium permanganate, treating at 22-27 degrees C for 120 hours, and washing with acidic solution to obtain graphene oxide, (b) mixing zinc chloride and graphene oxide, and treating with water and sodium hydroxide solution at 87-93 degrees C for 6 hours to obtain composite composition of zinc oxide and graphene oxide, and (c) annealing the composite composition. USE - The method is useful for producing composite composition of zinc oxide and graphene oxide (claimed). ADVANTAGE - The composition has high antibacterial ability. DETAILED DESCRIPTION - Producing composite composition, comprises either: (a) mixing 100 pts. wt. sodium nitrate, 430-460 pts. wt. sulfuric acid and 580-600 pts. wt. potassium permanganate, treating at 22-27 degrees C for 120 hours, and washing with acidic solution to obtain graphene oxide, (b) mixing zinc chloride and graphene oxide, and treating with water and sodium hydroxide solution at 87-93 degrees C for 6 hours to obtain composite composition of zinc oxide and graphene oxide, and (c) annealing the composite composition; or (i) mixing 100 pts. wt. sulfuric acid and 1-3 pts. wt. hydrogen peroxide, treating at 92-97 degrees C for 120 hours, washing with acidic solution to obtain graphene oxide, (ii) mixing zinc chloride and graphene oxide, treating with water and sodium hydroxide solution at 87-90 degrees C for 6 hours to obtain composite composition of zinc oxide and graphene oxide, and (iii) annealing the composite composition of zinc oxide and graphene oxide. An INDEPENDENT CLAIM is also included for composite composition produced by the above method.