• 专利标题:   Preparation of boron-doped graphene quantum dots used for detecting iron ions, involves hydrothermally reacting mixed solution of 1,3,6-trinitropyrene and borax, purifying by dialysis, and freeze-drying.
  • 专利号:   CN107586540-A
  • 发明人:   XI F, GE S, SHEN C, JIANG X, HUANG B
  • 专利权人:   UNIV ZHEJIANG SCI TECH
  • 国际专利分类:   B82Y020/00, B82Y030/00, B82Y040/00, C09K011/65, G01N021/64, G01N021/78
  • 专利详细信息:   CN107586540-A 16 Jan 2018 C09K-011/65 201817 Pages: 11 Chinese
  • 申请详细信息:   CN107586540-A CN10757366 29 Aug 2017
  • 优先权号:   CN10757366

▎ 摘  要

NOVELTY - Preparation of boron-doped graphene quantum dots, involves hydrothermally reacting a mixed solution of 1,3,6-trinitropyrene and borax, purifying by dialysis, and freeze-drying. USE - Preparation of boron-doped graphene quantum dots used for detecting iron ions (all claimed). ADVANTAGE - The method provides boron-doped graphene quantum dots which can emit yellow fluorescence, and has excellent fluorescent stability (fluorescence intensity remains 99% of the initial fluorescence intensity even when left for 3 months), peroxidase activity to catalyze hydrogen peroxide oxidation of 3,5,3',5'-tetramethylbenzidine color development reaction, and selective identification ability with respect to iron ions. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for boron-doped graphene quantum dots having a thickness of 1.2-1.8 nm and a grain size of 2-4 nm.