• 专利标题:   Preparation of graphene comprises soaking graphite powder or crystalline flake into mixed acid solution, adding polar intercalating agent, stirring, washing with water, drying, dispersing obtained graphite, and ultrasound crushing.
  • 专利号:   CN102431998-A
  • 发明人:   WU H
  • 专利权人:   SHENZHEN CHANGYIJINGXIN INVESTMENT CO
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN102431998-A 02 May 2012 C01B-031/04 201323 Pages: 11 Chinese
  • 申请详细信息:   CN102431998-A CN10278999 20 Sep 2011
  • 优先权号:   CN10278999

▎ 摘  要

NOVELTY - A graphene is prepared by soaking graphite powder or crystalline flake into mixed acid solution, adding polar intercalating agent, and stirring for 6-24 hours; washing with water, where mixture has pH of 5-7, and drying at 60 degrees C; drying sample at 600-1000 W microwave power of microwave apparatus for 0.5-2 minutes; and dispersing obtained graphite in water or organic solvent, and ultrasound crushing for 10-40 minutes to obtain desired graphene. USE - Method for preparation of graphene. ADVANTAGE - The method has low cost, high yield, simple and easy preparation, and low energy consumption, and is suitable for large scale production.