• 专利标题:   Preparation of graphene gel by adding graphite oxide to solvent, ultrasonically dispersing, heating to obtain graphene wet gel, placing into autoclave, reacting, slowly taking out to release high-pressure hot steam, and drying.
  • 专利号:   CN103896256-A
  • 发明人:   WANG Y, WU F, YUAN X, ZHOU M
  • 专利权人:   OCEANS KING LIGHTING SCI TECHNOLOGY CO, SHENZHEN OCEANS KING LIGHTING ENG CO LTD, SHENZHEN OCEANS KING LIGHTING SCI TECH
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN103896256-A 02 Jul 2014 C01B-031/04 201460 Pages: 6 Chinese
  • 申请详细信息:   CN103896256-A CN10574015 26 Dec 2012
  • 优先权号:   CN10574015

▎ 摘  要

NOVELTY - Preparation of graphene gel comprises adding graphite oxide to solvent, ultrasonically dispersing to obtain 2-10 mg ml graphene oxide suspension, placing into graphite oxide reactor, sealing, and heating to 150-200 degrees C for 2-10 hours to obtain graphene wet gel; and placing into autoclave, reacting to 200-400 degrees C at 5-25 MPa for 10-60 seconds, slowly taking out to release high-pressure hot steam, and drying. USE - Method for preparation of graphene gel (claimed). ADVANTAGE - The method utilizes supercritical solvent, eliminates the presence of solvent capillary force, and avoids the collapse of gel structure.