• 专利标题:   Three-dimensional graphene load molybdenum disulfide nano-mesh structure material comprises molybdenum disulfide nano-homogenously loaded on three dimensional graphene network.
  • 专利号:   CN107774282-A
  • 发明人:   HE C, DIAO Y, ZHAO N, SHI C, LIU E, HE F, MA L, LI J
  • 专利权人:   UNIV TIANJIN
  • 国际专利分类:   B01J027/051, C25B001/04, C25B011/06, B82Y030/00, B82Y040/00
  • 专利详细信息:   CN107774282-A 09 Mar 2018 B01J-027/051 201825 Pages: 8 Chinese
  • 申请详细信息:   CN107774282-A CN10791716 05 Sep 2017
  • 优先权号:   CN10791716

▎ 摘  要

NOVELTY - A three-dimensional graphene load molybdenum disulfide nano-mesh structure material comprises molybdenum disulfide nano-homogenously loaded on three dimensional graphene network. The molybdenum disulfide is 50-200 nm thick. The three-dimensional graphene is 1-10 nm thick. USE - Three-dimensional graphene load molybdenum disulfide nano-mesh structure material. ADVANTAGE - The structure material has wide availability of raw material and high burning heat value and environment-friendly. It is clean and used as renewable fossil fuel substitute. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for a preparation method of the three-dimensional graphene load molybdenum disulfide nano-mesh structure material which comprises: (A) mixing sucrose, glucose, citric acid, ammonium citrate, and starch as carbon source, using paratungstate tetrahydrate ammonium molybdate as molybdenum source; (B) adding carbon source, molybdenum source and sodium sulfate into deionized water to dissolve, stirring to prepare solution, ultrasonically mixing, carrying out spray drying to obtain precursor, and spraying at 105-220 degrees C; (C) grinding precursor into powder, laying in ark, calcining in tubular furnace, and introducing 200-400 ml/minute inert gases to remove air to flow; (D) taking argon as carrier gas, heating tubular furnace to 650-800 degrees C, carbonizing, cooling to room temperature after reaction is finished, and obtaining calcined product; and (E) collecting calcined product, grinding, water washing, calcining product without sodium hydroxide t 60-120 degrees C and drying.