• 专利标题:   Preparing graphene three dimensional printing material for three dimensional printing wires, involves preparing raw materials, removing tetrahydrofuranby distillation to separate the water into two parts A and B.
  • 专利号:   CN110527221-A
  • 发明人:   DENG Z
  • 专利权人:   MINDRUN SUNWAY PROTOTYPES CHANGZHOU CO
  • 国际专利分类:   B33Y070/00, C08K003/04, C08K003/36, C08L027/06, C08L035/00
  • 专利详细信息:   CN110527221-A 03 Dec 2019 C08L-027/06 201999 Pages: 5 Chinese
  • 申请详细信息:   CN110527221-A CN10972464 14 Oct 2019
  • 优先权号:   CN10972464

▎ 摘  要

NOVELTY - Preparing graphene three dimensional (3D) printing material involves preparing raw materials of 10-20 pts. wt. polyvinyl chloride, 10-40 pts. wt. silica gel powder, 10-30 pts. wt. graphene, 1-3 pts. wt. maleic anhydride polymer, and 80-100 pts. wt. tetrahydrofuran. The tetrahydrofuran is removed by distillation to separate the water into two parts A and B. The mass ratio of the A solution to the B solution is (2-3):1. The silica gel powder is put in solution A, stirred until dissolved, and then dispersed the graphene. After mixing the polyvinyl chloride and maleic anhydride polymers, put them into the B solution to fully dissolve them. After mixing the two solutions at 30-60 degrees C, warmed up to 120 degrees C until the reaction is complete, and collected the volatile tetrahydrofuran. The solution is cryogenically powder to obtain a 3D printing material with a powder diameter of 20-200 nanometer. USE - Method for preparing graphene 3D printing material used for 3D printing wires. ADVANTAGE - The method enables to prepare graphene 3D printing material for 3D printing wires, that can be made to realize the diversification of material applications.