• 专利标题:   Preparation of graphene oxide film, involves cleaning ceramic tube substrate surface, glazing, calcining, rubbing and coating (alpha)-alumina powder-containing aqueous solution on surface of ceramic tube substrate.
  • 专利号:   CN107226719-A
  • 发明人:   WU S, YANG H
  • 专利权人:   UNIV SOUTH CHINA TECHNOLOGY
  • 国际专利分类:   C04B041/89, C07C029/76, C07C031/20
  • 专利详细信息:   CN107226719-A 03 Oct 2017 C04B-041/89 201777 Pages: 10 Chinese
  • 申请详细信息:   CN107226719-A CN10332376 12 May 2017
  • 优先权号:   CN10332376

▎ 摘  要

NOVELTY - The preparation of graphene oxide film involves (i) cleaning the surface of a ceramic tube substrate, glazing, calcining, rubbing and coating different particle sized ( alpha )-alumina powder-containing aqueous solution on the surface of ceramic tube substrate, calcining to obtain smooth surfaced ceramic tube substrate, (ii) sealing the ceramic tube ends with PTFE stopper, vertically immersing in graphene oxide solution, removing, naturally drying, immersing in graphene oxide aqueous solution, repeating for 2-10 times, and leaving still the mixture at room temperature in air atmosphere. USE - Preparation of graphene oxide film (claimed). ADVANTAGE - The method enables the preparation of graphene oxide film quickly and easily with high yield, uniform morphology, excellent smoothness, stability, and separation effect, and controllable flux and separation factor. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for application of graphene oxide film in dehydration of high-concentration ethylene glycol solution, which involves using graphene oxide film as a separation membrane, pervaporating, and dehydrating high-concentration ethylene glycol.