• 专利标题:   Preparation graphene-molybdenum disulfide composite used for adsorbing organic contaminants in water, involves weighing graphite oxide in container containing water, mixing with sodium molybdate dihydrate and putting in ultrasonicator.
  • 专利号:   CN106378096-A
  • 发明人:   ZHAO H, HAO S, ZHU P, LI T, MAO Z, KAI L
  • 专利权人:   UNIV NANJING MEDICAL
  • 国际专利分类:   B01J020/20, B01J020/30, C02F001/28, C02F101/30
  • 专利详细信息:   CN106378096-A 08 Feb 2017 B01J-020/20 201732 Pages: 9 Chinese
  • 申请详细信息:   CN106378096-A CN11039254 21 Nov 2016
  • 优先权号:   CN11039254

▎ 摘  要

NOVELTY - Preparation graphene-molybdenum disulfide composite involves weighing 50-65 milligram graphite oxide in container containing 40-55 milliliter water, mixing with 0.3-0.8 gram sodium molybdate dihydrate and putting in ultrasonicator for 20-30 minutes to obtain suspension. The suspension is adjusted at pH 6-6.5 by adding 0.1-0.3 mol per liter sodium hydroxide solution and added 0.6-1 gram thioacetamide to obtain a mixed solution. The mixed solution is transferred to polytetrafluoroethylene reactor and allowed to stand at 180-250 degrees C for 15-30 hours to obtain reaction solution. USE - Method for preparing graphene-molybdenum disulfide composite used for adsorbing organic contaminants in water (all claimed). ADVANTAGE - The method enables to prepare graphene-molybdenum disulfide composite in simple and eco-friendly manner and has good absorption. DETAILED DESCRIPTION - Preparation graphene-molybdenum disulfide composite involves weighing 50-65 milligram graphite oxide in container containing 40-55 milliliter water, mixing with 0.3-0.8 gram sodium molybdate dihydrate and putting in ultrasonicator for 20-30 minutes to obtain suspension. The suspension is adjusted at pH 6-6.5 by adding 0.1-0.3 mol per liter sodium hydroxide solution and added 0.6-1 gram thioacetamide to obtain a mixed solution. The mixed solution is transferred to polytetrafluoroethylene reactor and allowed to stand at 180-250 degrees C for 15-30 hours to obtain reaction solution. The reaction solution is cooled and centrifuged to obtain precipitate and supernatant liquid. The supernatant liquid is removed and washed precipitate with deionized water for 5-6 times. The precipitate is dried at 60-80 degrees C for 7-8 hours to obtain graphene-molybdenum disulfide composite.