• 专利标题:   Preparing composite catalyst used for degrading organic matter comprising terramycin, involves reacting manganese source, cobalt source, dopamine and graphene oxides by hydrothermal method, calcining to obtain 3D-structure loaded with cobalt manganese oxide, N-doped reducing graphene oxide aerogel.
  • 专利号:   CN115532296-A
  • 发明人:   REN F, WANG Y, WANG C, YANG H, QU Y, TANG X, ZHU H, DING Y
  • 专利权人:   LANRUN ENVIRONMENTAL PROTECTION TECHNOLO, UNIV LANZHOU
  • 国际专利分类:   B01J023/889, B01J027/24, B01J035/10, C02F001/72, C02F101/34, C02F101/36, C02F101/38, C02F103/34
  • 专利详细信息:   CN115532296-A 30 Dec 2022 B01J-027/24 202315 Chinese
  • 申请详细信息:   CN115532296-A CN11204197 29 Sep 2022
  • 优先权号:   CN11204197

▎ 摘  要

NOVELTY - Preparing composite catalyst involves preparing graphene oxides (GOs) by Hummer method; taking manganese source, cobalt source, dopamine and prepared GO as raw material, where amount ratio of cobalt and manganese source is 1:2; performing hydrothermal method at 160-200℃ and heat preservation for 10-14 hours to obtain composite hydrogel; freezing and drying composite hydrogel to obtain composite aerogel; calcining at 500-700℃ and heat preservation for 3-5 hours to obtain three-dimensional (3D) structure, loaded with cobalt manganese oxide, N-doped reducing graphene oxide aerogel (3D-CoMn2O4/N-rGA). USE - Method for preparing composite catalyst used for degrading organic matter comprising terramycin, gatifloxacin and ibuprofen (claimed). ADVANTAGE - The method is simple, low raw material cost, short preparation period, quickly and efficiently activate phenylmethanesulfonic acid (PMS) to generate free radical, and avoid CoMn2O4dissolution and agglomeration. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for a composite catalyst, whhich has three-dimensional structure, loaded with cobalt manganese oxide (CoMn2O4), N-doped reducing graphene oxide aerogel.