• 专利标题:   Method for preparing lithium ion anode composite material of nitrogen-doped graphene/silicon three-dimensional structure, involves reacting solution to dry product that is subjected to high temperature treatment to obtain final product.
  • 专利号:   CN108615860-A
  • 发明人:   WEN G, TANG J
  • 专利权人:   UNIV SHANDONG TECHNOLOGY
  • 国际专利分类:   H01M004/36, H01M004/38, H01M004/62, H01M010/0525
  • 专利详细信息:   CN108615860-A 02 Oct 2018 H01M-004/36 201875 Pages: 10 Chinese
  • 申请详细信息:   CN108615860-A CN10215307 15 Mar 2018
  • 优先权号:   CN10215307

▎ 摘  要

NOVELTY - The method involves dispersing the nano silicon powder in water, and adding polydially dimethyl-ammonium chloride (PDDA) for stirring and ultrasonic reaction. The obtained solution is subjected to washing and centrifugation to obtain PDDA-silicon (Si) product. The obtained PDDA-Si product is added to the aqueous graphene oxide solution, and is stirred and ultrasonicated. The formaldehyde is added and stirred. The melamine is added and stirred. The final solution is hydrothermally reacted to dry the product after the hydrothermal reaction. The dried product is subjected to high temperature treatment to obtain a product. USE - Method for preparing lithium ion anode composite material of nitrogen-doped graphene/silicon three-dimensional structure. ADVANTAGE - The surface activation energy of nano-silicon particles can be changed. The problem of nano-silicon particles easy to agglomerate and difficult to disperse is alleviated. The nitrogen atom is introduced by the hydrothermal reaction, while reducing the graphene oxide to obtain nitrogen-doped graphene. DESCRIPTION OF DRAWING(S) - The drawing shows a photographic view of the material prepared by preparing nitrogen-doped graphene/silicon three-dimensional lithium ion negative electrode composite material.