• 专利标题:   Preparing cadmium sulfide/copper oxide/graphene photocathode protective composite material comprises e.g. dispersing graphene oxide in copper nitrate solution, adding urea solution, carrying out hydrothermal reaction and calcining.
  • 专利号:   CN108286050-A
  • 发明人:   YAO C, CHEN J, ZUO S, LIU W, LI X, LIU Z
  • 专利权人:   UNIV CHANGZHOU
  • 国际专利分类:   C23F013/12
  • 专利详细信息:   CN108286050-A 17 Jul 2018 C23F-013/12 201853 Pages: 8 Chinese
  • 申请详细信息:   CN108286050-A CN10033142 14 Jan 2018
  • 优先权号:   CN10033142

▎ 摘  要

NOVELTY - Preparing cadmium sulfide/copper oxide/graphene photocathode protective composite material comprises (i) dispersing graphene oxide in copper nitrate solution, adding urea solution, stirring, carrying out hydrothermal reaction, cooling, filtering, drying filter cake and calcining under nitrogen atmosphere to obtain copper oxide/graphene composite material, and (ii) dispersing copper oxide/graphene composite material prepared in step (i) in aqueous solution of cadmium salt, adding thiourea, stirring under ice bath, adjusting the pH value, then adding aqueous solution of sodium sulfide, stirring under dark condition, filtering, washing filter cake and drying to obtain cadmium sulfide/copper oxide/graphene composite material. USE - The composite material is useful for anti-corrosion metal under dark environment (claimed). DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for cadmium sulfide/copper oxide/graphene photocathode protective composite material is obtained by above method.