• 专利标题:   Synthesis of graphene material by mixing dodecylamine-ethanol, ferrous chloride and ammonium dihydrogen phosphate, centrifuging, adding phenol-ethanol solution, calcining, treating with hydrochloric acid, washing, and vacuum drying.
  • 专利号:   CN103738959-A, CN103738959-B
  • 发明人:   HU M, MAO L, PAN B, GAO S, GUO X
  • 专利权人:   UNIV NANJING
  • 国际专利分类:   B82Y030/00, B82Y040/00, C01B031/04
  • 专利详细信息:   CN103738959-A 23 Apr 2014 C01B-031/04 201439 Pages: 8 Chinese
  • 申请详细信息:   CN103738959-A CN10056369 19 Feb 2014
  • 优先权号:   CN10056369

▎ 摘  要

NOVELTY - A graphene material is synthesized by mixing dodecylamine-ethanol, ferrous chloride and ammonium dihydrogen phosphate at 45-55 degrees C, centrifuging, drying, grinding, putting in crucible at 40-60 degrees C, vacuum drying for 12-36 hours, adding phenol-ethanol solution, mixing, vacuum drying at 40-60 degrees C for 12-72 hours, calcining in tubular furnace under argon protective atmosphere at 600-900 degrees C for 6-24 hours, treating with concentrated hydrochloric acid, heating at 160-200 degrees C for 24-48 hours, centrifuging, washing by water or anhydrous ethanol, and vacuum drying at 40-60 degrees C for 12-24 hours. USE - Method for synthesizing graphene material (claimed). ADVANTAGE - The method is simple and fast.