• 专利标题:   Preparation of elastic and conductive aerogel for e.g. elastic sensor, involves adding formaldehyde to resorcinol solution, adding graphene oxide dispersion, aging, extracting, drying and carbonizing.
  • 专利号:   CN105271193-A, CN105271193-B
  • 发明人:   FU Z, WANG C, ZHANG L, ZHAO H, WU W, YANG X, YUAN L, ZHU J, MI R, ZHONG M
  • 专利权人:   LASER FUSION RES CENT CHINA ACAD ENG PHY, LASER FUSION RES CENT CHINA ACAD ENG PHY
  • 国际专利分类:   C01B031/04, C01B032/194
  • 专利详细信息:   CN105271193-A 27 Jan 2016 C01B-031/04 201643 Chinese
  • 申请详细信息:   CN105271193-A CN10683871 20 Oct 2015
  • 优先权号:   CN10683871

▎ 摘  要

NOVELTY - Preparation of elastic and conductive aerogel with ultralow density and ultrahigh specific surface area involves mixing resorcinol and deionized water, stirring, adding formaldehyde solution and sodium carbonate, stirring for 15-30 minutes, adding graphene oxide dispersion, adding dispersion to a closed vessel, maintaining at 60-80 degrees C for 3-15 days to obtain a hydrogel, acidifying, aging, performing solvent exchange, extracting, drying, carbonizing and cooling to room temperature. USE - Preparation of elastic and conductive aerogel for elastic sensor, separation and adsorption materials, electrode materials and hydrogen storage materials. ADVANTAGE - The elastic and conductive aerogel with ultralow density and ultrahigh specific surface area is produced economically. DETAILED DESCRIPTION - Preparation of elastic and conductive aerogel with ultralow density and ultrahigh specific surface area involves mixing resorcinol and deionized water in weight ratio of 1:5-80, stirring, adding formaldehyde solution, stirring for 15-30 minutes, adding sodium carbonate, stirring for 15-30 minutes, adding graphene oxide dispersion, adding dispersion to a closed vessel, maintaining at 60-80 degrees C for 3-15 days to obtain a hydrogel, acidifying, aging for 6-8 days, performing solvent exchange with acetone, extracting with supercritical carbon dioxide, drying to obtain organic aerogel, carbonizing at 150 degrees C for 2 hours, increasing temperature to 200-300 degrees C for 25-35 minutes, heating at 400-600 degrees C for 30-60 minutes, 700-800 degrees C for 1-2 hours and 900-1100 degrees C for 1-3 hours, and cooling to room temperature.