• 专利标题:   Method for preparing graphene/alpha nickel hydroxide nanometer composite material, involves preparing oxide aqueous solution, performing chemical reduction by aqueous solution, and mixing and reflowing nickel and urea in alcohol solvent.
  • 专利号:   CN102683040-A
  • 发明人:   MA P, ZHANG L, ZHANG W, ZHANG X
  • 专利权人:   UNIV ZHEJIANG
  • 国际专利分类:   H01G009/042
  • 专利详细信息:   CN102683040-A 19 Sep 2012 H01G-009/042 201310 Pages: 7 Chinese
  • 申请详细信息:   CN102683040-A CN10151522 16 May 2012
  • 优先权号:   CN10151522

▎ 摘  要

NOVELTY - A graphene/alpha nickel hydroxide nanometer composite material preparing method involves preparing a graphite oxide aqueous solution by dissolving graphite oxide in water, performing ultrasonic oscillation and adjusting pH value to 10. Chemical reduction is performed by using the graphite oxide aqueous solution with hydrazine hydrate, refluxing and stirring the mixture to obtain graphene. The reduced graphene, divalent soluble nickel and urea (4 mol/l) are mixed and reflowed in water alcohol solvents followed by refluxing and stirring, washing and drying to obtain finished product. USE - Method for preparing graphene/alpha nickel hydroxide nanometer composite material. ADVANTAGE - The method enables preparing composite material with excellent electrochemical property, high production efficiency and short period in a simple manner. DETAILED DESCRIPTION - A graphene/alpha nickel hydroxide nanometer composite material preparing method involves preparing a graphite oxide aqueous solution by dissolving graphite oxide (0.05-0.2%) in water, performing ultrasonic oscillation and adjusting the pH value to 10. Chemical reduction is performed by using the graphite oxide aqueous solution with hydrazine hydrate (80%) at ratio of 1:100, refluxing and stirring the mixture at 80-100 degrees C for 5-24 hours to obtain graphene. The reduced graphene, divalent soluble nickel and urea (4 mol/l) are mixed and reflowed in water alcohol solvents (5 g/l) followed by refluxing and stirring at 100 degrees C for 3-5 minutes, washing and drying to obtain finished product.