• 专利标题:   Preparation method of graphene nylon fiber, involves placing graphene in grinding mill, adding water, adding surface treating agent, and grinding to obtain graphene slurry, placing graphene slurry into container, and leaving still.
  • 专利号:   CN106498537-A
  • 发明人:   GE C, YAN H, GE X
  • 专利权人:   SHANGHAI HUALY SUPERFINES SCI TECHN CO
  • 国际专利分类:   D01F001/09, D01F001/10, D01F006/90
  • 专利详细信息:   CN106498537-A 15 Mar 2017 D01F-006/90 201735 Pages: 6 Chinese
  • 申请详细信息:   CN106498537-A CN10888499 11 Oct 2016
  • 优先权号:   CN10888499

▎ 摘  要

NOVELTY - The preparation method of graphene nylon fiber involves placing graphene in a grinding mill, adding water, adding surface treating agent, and grinding to obtain graphene slurry, placing graphene slurry into a container, leaving still, and taking out slurry in upper portion of container as graphene sheet dispersion slurry, passing graphene sheet dispersion slurry through 5-micron screen, pumping into a synthesis reaction kettle containing caprolactam, synthesizing to obtain graphene nylon chips, mixing graphene nylon chips and nylon chips, drying, and performing wire drawing process. USE - Preparation method of graphene nylon fiber (claimed). ADVANTAGE - The method enables preparation of graphene nylon fiber with excellent consistency, conductivity, electromagnetic wave resistance, antistatic property, and high efficient far infrared ray shielding properties. DETAILED DESCRIPTION - The preparation method of graphene nylon fiber involves (1) placing 10 wt.% graphene with particle size of less than or equal to 0.5 microns in a vertical grinding mill, adding deionized water, adding surface treating agent within 1 hour after grinding for 2-4 hours under action of grinding medium, and continuously grinding for 1 hour to obtain graphene slurry, placing the graphene slurry into a container, leaving still for 4 hours, and taking out the slurry in upper portion of the container as graphene sheet dispersion slurry, (2) passing the graphene sheet dispersion slurry through 5-micron screen, pumping into a synthesis reaction kettle containing caprolactam, synthesizing to obtain graphene nylon chips containing 0.5-3 wt.% graphene, and (3) uniformly mixing graphene nylon chips and nylon chips, drying, and performing wire drawing process, where the graphene nylon fiber contains 0.5-3 wt.% graphene.