• 专利标题:   Forming an electrode, comprises degreasing an electrode material, and coating the degreased electrode material with a liquid mixture, where the mixture comprises a dispersion of a graphene-type material in an organic solvent.
  • 专利号:   WO2012167218-A2, WO2012167218-A3, KR2014100930-A, IN201310391-P4
  • 发明人:   NICKEL C S, POWELL C E, BEALL G W
  • 专利权人:   DXUPCLOSE, UNIV TEXAS STATE, DXUPCLOSE, UNIV TEXAS STATE
  • 国际专利分类:   C12Q001/02, G01N015/10, G01N027/30, C12Q001/04, C12Q001/06, G01N027/00, G01N027/04
  • 专利详细信息:   WO2012167218-A2 06 Dec 2012 G01N-027/30 201301 Pages: 66 English
  • 申请详细信息:   WO2012167218-A2 WOUS040645 03 Jun 2012
  • 优先权号:   US493152P, KR700229

▎ 摘  要

NOVELTY - The method comprises degreasing an electrode material, and coating the degreased electrode material with a liquid mixture. The mixture comprises a dispersion of a graphene-type material in an organic solvent. The graphene-type material comprises hydroxyl groups. The graphene-type material is made of humic acid using catalytic hydrogenation, where the humic acid is extracted from leonardite. The catalytic hydrogenation includes a catalyst, and is conducted in a Parr reactor at 160 degrees C. A reaction product of the catalytic hydrogenation is passed through an acidic ion exchange column. USE - The method is useful for forming an electrode, which is useful in a sensor (claimed) for identifying microbes and counting microbes and determining antimicrobial sensitivity. ADVANTAGE - The method allows rapid and economical formation of the electrode with high conductivity and sensitivity thus providing simple, automatic, accurate and rapid detection of microbes. DETAILED DESCRIPTION - The method comprises degreasing an electrode material, and coating the degreased electrode material with a liquid mixture. The mixture comprises a dispersion of a graphene-type material in an organic solvent. The graphene-type material comprises hydroxyl groups, and is made of humic acid using catalytic hydrogenation, where the humic acid is extracted from leonardite. The catalytic hydrogenation includes a catalyst, and is conducted in a Parr reactor at 160 degrees C. A reaction product of the catalytic hydrogenation is passed through an acidic ion exchange column. The electrode material includes a metal, a metal salt, or a metal oxide. The step of degreasing includes treating the electrode material with the organic solvent. The coating includes dip coating, spray coating, brush coating, stamp coating, lithographic coating and/or UV light lithographic coating. The graphene-type material is present in the dispersion at a concentration of less than 1.8-2.5 wt.% An INDEPENDENT CLAIM is included for a sensor.