• 专利标题:   Temperature-controllable surface boiling coating device for boiling and depositing three-dimensional structure on curved surface, has nickel-chromium alloy wire that is fixed in device by controlling boiling solution temperature.
  • 专利号:   CN114717553-A
  • 发明人:   TAO P, SHANG W, DENG T, TAO J, ZHANG W, CHENG W, CHU B, FU B, FANG C
  • 专利权人:   UNIV SHANGHAI JIAOTONG
  • 国际专利分类:   B01F033/452, C23C026/00
  • 专利详细信息:   CN114717553-A 08 Jul 2022 C23C-026/00 202270 Chinese
  • 申请详细信息:   CN114717553-A CN10318993 29 Mar 2022
  • 优先权号:   CN10318993

▎ 摘  要

NOVELTY - The device has a double-layer cylinder container (1), a positioning device (5), a fixing device (6), and a platinum plate electrode clip (7) all placed on the magnetic stirring device (8). The platinum plate electrode clip is vertically suspended and arranged by the positioning device and the fixing device. The platinum plate electrode clip straightens the nickel-chromium alloy wire (10) and places horizontally. The thermocouple (11) is positioned in the inner cylinder of the double-layer cylinder through the positioning device. The digital display interface of the thermocouple is placed on one side of the double-layer cylinder. The stirring magnet (9) is placed in the inner cylinder of the double-layer cylinder. The outer layer of the double-layer tank container, the temperature-controlled water bath (2), and the conduit connection constitute a circulation loop. The power supply device (3) is connected to the platinum electrode clip through copper wires. USE - Temperature-controllable surface boiling coating device for boiling and depositing three-dimensional structure on curved surface used in fields of aerospace and civil automobiles. ADVANTAGE - The device adopts double-layer cylinder container and the temperature control water bath to form accurate and stable temperature control, without using the heating substrate placed at the bottom of the container for preheating, so that the boiling precursor solution whole temperature distribution is uniform. The device effectively avoids the problem of solute reunion and unstable caused by over-high temperature of the solution during the boiling and depositing process. The nickel-chromium alloy wire curved surface is uniformly distributed by non-template boiling deposition method, which has stable structure of three-dimensional structure graphene film, and greatly improves the surface nuclear boiling heat transfer application of bubble-shaped core and boiling performance. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for a surface boiling deposition three-dimensional structure method based on the temperature-controllable surface boiling coating device, which involves alkali washing the nickel-chromium alloy wire in sodium hydroxide solution at room temperature, removing oxide layer in dilute sulfuric acid solution, and washing with acetone and deionizing water respectively, uniformly dispersing the graphene oxide powder in deionized water, adding a surface stabilizer to form a stable dispersion of graphene oxide, dissolving by magnetic stirring to form a uniform and stable boiling precursor solution, where the surface stabilizer is the surface stabilizer of ammonium ions, installing the nickel-chromium alloy wire, pouring the boiling precursor solution into the inner layer of the double-layer cylinder container, connecting a temperature-controlled water bath to the outer layer of the double-layered tank container through a conduit, and controlling the temperature of the water bath, turning on the magnetic stirring device, stirring the boiling precursor solution, and adjusting the rotational speed of the magnetic stirring device, connecting the positive and negative poles of the power supply device to the two platinum electrode clips respectively, and turning on the power supply, adjusting the voltage input, and calculating the input heating power according to the current value measured and fed back by the power supply equipment, turning off the power supply of the power supply equipment in turn, disconnecting the wire connection with the platinum electrode clip, turning off the temperature-controlled water bath, removing the nichrome wire deposited by boiling, rinsing with deionized water, and drying naturally. DESCRIPTION OF DRAWING(S) - The drawing shows the structure schematic diagram of a surface boiling coating device with controllable temperature. 1Double-layer cylinder container 2Temperature-controlled water bath 3Power supply device 4Conduit 5Positioning device 6Fixing device 7Platinum plate electrode clip 8Magnetic stirring device 9Stirring magnet 10Nickel-chromium alloy wire 11Thermocouple