• 专利标题:   Method for preparing polyurethane-modified graphene microchips comprises e.g. adding graphene oxide and polyol into three-necked flask, stirring, and simultaneously performing high-temperature vacuum dehydration and adding isocyanate.
  • 专利号:   CN112608436-A, WO2022127745-A1, AU2021402785-A1
  • 发明人:   FENG Z, WANG Y, LIU L, KANG Y, LI D, QIN W, WU D
  • 专利权人:   WUHAN MATERIAL PROTECTION RES INST MIN, WUHAN RES INST MATERIALS PROTECTION, WUHAN RES INST MATERIALS PROTECTION
  • 国际专利分类:   C08G018/32, C08G018/44, C08G018/48, C08K003/04, C09D163/00, C09D175/04, C09D005/08, C09D007/62
  • 专利详细信息:   CN112608436-A 06 Apr 2021 C08G-018/48 202136 Pages: 12 Chinese
  • 申请详细信息:   CN112608436-A CN11476438 14 Dec 2020
  • 优先权号:   CN11476438

▎ 摘  要

NOVELTY - Method for preparing polyurethane-modified graphene microchips comprises (i) adding graphene oxide and polyol into a three-necked flask, stirring and mixing, and simultaneously performing high-temperature vacuum dehydration; (ii) high-temperature vacuum dehydrating, mixing and stirring, stopping heating, controlling the reaction temperature to cool to room temperature, and gradually adding isocyanate, monitoring the reaction temperature, adjusting the addition rate according to the reaction temperature, and controlling the reaction temperature to less than T degrees C; and (iii) adding isocyanate, reacting for 10-30 minutes, controlling the reaction temperature within the range of 75-85 degrees C by heating in an oil bath, stirring the reaction for 1.5-3 hours, and using a filter to filter and encapsulate to complete the preparation of polyurethane modified graphene microchips. USE - The method is useful for preparing polyurethane-modified graphene microchips. ADVANTAGE - The microchip greatly improves the corrosion resistance of the coating. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for polyurethane-modified graphene microchip prepared by the above mentioned method.