• 专利标题:   Composite hydrogel, useful for adsorption of heavy metal ions in industrial wastewater, comprises polyethylene alcohol, chitosan, modified graphene oxide, and sodium alginate, where the modified graphite oxide is ferroferric oxide.
  • 专利号:   CN104226281-A, CN104226281-B
  • 发明人:   MA P, CHEN M, JIN J, LI K, HUANG Y, DONG W, LI L, FU M, HU Y
  • 专利权人:   UNIV JIANGNAN
  • 国际专利分类:   B01J020/26, B01J020/28, B01J020/30, C02F001/28, C02F001/62
  • 专利详细信息:   CN104226281-A 24 Dec 2014 B01J-020/26 201513 Pages: 17 Chinese
  • 申请详细信息:   CN104226281-A CN10540016 13 Oct 2014
  • 优先权号:   CN10540016

▎ 摘  要

NOVELTY - Composite hydrogel comprises polyethylene alcohol, chitosan, modified graphene oxide, and sodium alginate. The modified graphite oxide is ferroferric oxide. USE - The composite hydrogel is useful for adsorption of heavy metal ions in industrial wastewater (all claimed). ADVANTAGE - The composite hydrogel can be simply and rapidly prepared with high adsorption capacity, good stability and strong operability. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for preparing the composite hydrogel, comprising adding the polyethylene alcohol, sodium alginate, and deionized water in a bottle and then mixing, stirring the mixture for 1-4 hours and heating to obtain mixed liquid, adding the mixed liquid in a water bath and then heating at temperature of 60-100 degrees C, adding chitosan and then stirring for 2-10 hours and cooling to room temperature, adding 1-5 pts. wt. modified graphene oxide and then stirring for 0.2-2 hours and dispersing, dropping the modified graphene oxide solution into calcium chloride-boric acid saturated solution and then reacting to obtain spherical hydrogel having a grain diameter size of 0.5-10 mm, soaking the spherical hydrogel with saturated solution for 12-36 hours and then flushing with 2-6 times of deionized water.