• 专利标题:   Quick green synthesized graphene oxide-modified popcorn-like silver SERS composite structure comprises silver nitrate, EDTA, stannous chloride, acetone, anhydrous ethanol, dilute sulfuric acid, and deionized water.
  • 专利号:   CN108411285-A
  • 发明人:   ZHANG M, CHEN Z, CHEN T
  • 专利权人:   UNIV HEFEI TECHNOLOGY
  • 国际专利分类:   C23C018/18, C23C018/16, C23C018/42, B82Y040/00, B82Y030/00
  • 专利详细信息:   CN108411285-A 17 Aug 2018 C23C-018/18 201862 Pages: 9 Chinese
  • 申请详细信息:   CN108411285-A CN10371961 24 Apr 2018
  • 优先权号:   CN10371961

▎ 摘  要

NOVELTY - Quick green synthesized graphene oxide-modified popcorn-like silver surface-enhanced Raman scattering (SERS) composite structure comprises 14-30 pts. wt. silver nitrate, 14-30 pts. wt. EDTA, 7-15 pts. wt. stannous chloride, 2-7 pts. wt. acetone, 5-15 pts. wt. anhydrous ethanol, 3-9 pts. wt. dilute sulfuric acid, and balance deionized water. USE - Quick green synthesized graphene oxide-modified popcorn-like silver SERS composite structure. ADVANTAGE - The structure is stable and uniform. The preparation method is repeatable. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for synthesizing the SERS composite structure comprising pretreating copper, ultrasonic washing with ethanol and deionized water for 2-3 minutes, adding dilute sulfuric acid for 4-6 minutes, washing with deionized water, adding stannous chloride solution, silver nitrate solution and EDTA, absorbing, tin for 10-12 minutes, removing acetone, drying, soaking in silver nitrate solution, and ultrasonic cleaning with deionized water and anhydrous ethanol.