• 专利标题:   Preparing multi-stage nanosheet array nickel cobaltite/reduced graphene oxide/nickel foam useful as electrode of methanol fuel cell and super capacitor, comprises e.g. dissolving cobalt nitrate hexahydrate in deionized water, and transferring slurry to Teflon reaction kettle.
  • 专利号:   CN115083798-A
  • 发明人:   LIU T, ZHAO Z, LIU H, JIANG M, ZHANG Q, WANG D, JIANG D, LI S, QU M
  • 专利权人:   FAW CAR CO LTD
  • 国际专利分类:   H01G011/30, H01G011/86
  • 专利详细信息:   CN115083798-A 20 Sep 2022 H01G-011/86 202298 Chinese
  • 申请详细信息:   CN115083798-A CN10472423 29 Apr 2022
  • 优先权号:   CN10472423

▎ 摘  要

NOVELTY - Method for preparing multi-stage nanosheet array nickel cobaltite/reduced graphene oxide/nickel foam comprises dissolving cobalt nitrate hexahydrate in deionized water to form a mixed salt solution, dripping a mixture salt solution and an alkali solution at a speed of 0.8-1.5 ml/minute to make a pH of the solution stable at 10-0.1, controlling pH of solution in a four-necked flask to be 0.1 and stabilizing for 6-9 minutes, mixing nickel nitrate and cobalt sulfate in deionized water to dissolve cobalt sulfate hexahydrate to obtain a mixed solution, transferring obtained slurry containing reduced graphene oxide/nickel foam to a Teflon(Polytetrafluoroethylene) reaction kettle, crystallizing at 85-95℃ for 5-7 hours, cooling, and washing obtained product with deionized water. USE - The method is useful for preparing multi-stage nanosheet array nickel cobaltite/reduced graphene oxide/nickel foam, which is useful as electrode of methanol fuel cell and super capacitor (claimed). ADVANTAGE - The method enables to prepare multi-stage nanosheet array nickel cobaltite/reduced graphene oxide/nickel foam, which has high conductivity graphene composite, and increases the active site exposure, which is more beneficial for electron or particle transmission. The nano-sheet has a porous structure, forming a large amount of open channel between the interconnected nano-sheets, and is beneficial for electrolyte ion penetration. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for multi-stage nanosheet array nickel cobaltite/reduced graphene oxide/nickel foam.