• 专利标题:   Preparing phase change microcapsule type heat absorbing agent comprises adding wall pre-polymer into silica-graphene oxide solution, reacting, adding into low melting paraffin emulsion, cooling, washing, vacuum drying and crushing.
  • 专利号:   CN108570310-A
  • 发明人:   PENG Z, FENG Q, HUO J, ZHENG Y, ZHANG J, LIU X
  • 专利权人:   UNIV SOUTHWEST PETROLEUM
  • 国际专利分类:   C09K005/06, C09K008/467
  • 专利详细信息:   CN108570310-A 25 Sep 2018 C09K-005/06 201876 Pages: 10 Chinese
  • 申请详细信息:   CN108570310-A CN10311624 09 Apr 2018
  • 优先权号:   CN10311624

▎ 摘  要

NOVELTY - Preparing phase change microcapsule type heat absorbing agent useful for cementing slurry, comprises: (i) adding amino group into nano silica using a modifier to obtain modified silica; (ii) dissolving modified silica and graphene oxide in water to obtain silica-graphene oxide solution; (iii) adding the prepared wall pre-polymer into silica-graphene oxide solution and reacting to obtain nano-material modified pre-polymer solution; (iv) preparing core material low melting paraffin emulsion; and (v) heating and stirring in a constant temperature water bath at 40 degrees C, drop-wisely adding the modified prepolymer solution into the low melting paraffin emulsion, adjusting the pH of the system to 3-4, heating to 65 degrees C, adding curing agent solution, cooling, washing, suction filtering, vacuum drying and crushing. USE - The method is useful for preparing phase change microcapsule type heat absorbing agent. ADVANTAGE - The heat absorbing agent overcomes the defect by phase change material.