• 专利标题:   Preparation of ZIF-8/graphene composite aerogel used in e.g. electrolysis of water for hydrogen evolution, involves mixing graphite powder and sodium nitrate, dripping into acid solution, reacting with e.g. manganese source, ultrasonically stirring, hydrothermally reacting, and calcining.
  • 专利号:   CN113774429-A
  • 发明人:   GUO Z, ZUO X, WANG J
  • 专利权人:   WUHAN INST TECHNOLOGY
  • 国际专利分类:   C25B001/04, C25B011/095
  • 专利详细信息:   CN113774429-A 10 Dec 2021 C25B-011/095 202234 Chinese
  • 申请详细信息:   CN113774429-A CN10964625 19 Aug 2021
  • 优先权号:   CN10964625

▎ 摘  要

NOVELTY - The preparation of ZIF-8/graphene composite aerogel, involves (S1) mixing graphite powder and sodium nitrate, dripping into acid solution, adding manganese source, stirring, washing and centrifuging to obtain graphene oxide solution, (S2) adding zinc source and dimethylimidazole aqueous solution to graphene oxide solution, ultrasonically stirring, placing in high-pressure reactor, hydrothermally reacting, and lyophilizing the product after reaction to obtain aerogel, and (S3) calcining aerogel in muffle furnace. USE - Preparation of ZIF-8/graphene composite aerogel used in electrolysis of water for hydrogen evolution (claimed). ADVANTAGE - The method enables preparation of ZIF-8/graphene composite aerogel by simple process, ensuring mild reaction conditions, and the prepared ZIF-8/graphene composite aerogel has stable structure and large number of active sites, which is beneficial to improve the efficiency of electrocatalytic hydrogen evolution.