• 专利标题:   Three-dimensional graphene is stratified, and gradually outwards is sleeved at outer side of inner layer graphene and is prepared by treating crystalline flake graphite with concentrated sulfuric acid and then with potassium permanganate.
  • 专利号:   CN106976869-A
  • 发明人:   ZHANG D, WANG Y
  • 专利权人:   UNIV TONGJI
  • 国际专利分类:   C01B032/184
  • 专利详细信息:   CN106976869-A 25 Jul 2017 C01B-032/184 201761 Pages: 9 Chinese
  • 申请详细信息:   CN106976869-A CN10281367 26 Apr 2017
  • 优先权号:   CN10281367

▎ 摘  要

NOVELTY - Three-dimensional graphene is stratified, and gradually outwards is sleeved at the outer side of the inner layer graphene. USE - Three-dimensional graphene. ADVANTAGE - The three-dimensional graphene has special sleeve-shaped structure, has excellent mechanical property, structural stability, has certain anisotropy on the direction vertical to the bottom surface and parallel bottom surface, electrical conductivity and thermal conductivity. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for a method for preparing three-dimensional graphene which involves: (A) adding crystalline flake graphite into concentrated sulfuric acid and stirring; (B) adding potassium permanganate, stirring uniformly; (C) adding de-ionized water and hydrogen peroxide solution; (D) filtering to obtain the precipitate; (E) washing to obtain graphite oxide; (F) ultrasonicating; (G) hydrothermally reducing graphite oxide to obtain three dimensional graphene hydrogel; and (H) freeze drying to obtain three-dimensional graphene.