• 专利标题:   Preparation of doped graphene involves cleaning metal material and drying, subjecting dried substrate in reaction chamber, introducing protective gas, heating, and introducing gaseous carbon-containing and nitrogen-containing materials.
  • 专利号:   CN103088312-A
  • 发明人:   WANG Y, YUAN X, ZHOU M
  • 专利权人:   OCEAN S KING LIGHTING SCI TECHNOLOGY, HAIYANGWANG LIGHTING TECHNOLOGY CO LTD
  • 国际专利分类:   C01B031/02, C23C016/26
  • 专利详细信息:   CN103088312-A 08 May 2013 C23C-016/26 201372 Pages: 7 Chinese
  • 申请详细信息:   CN103088312-A CN10343273 03 Nov 2011
  • 优先权号:   CN10343273

▎ 摘  要

NOVELTY - A doped graphene is prepared by cleaning metal material and drying, subjecting dried substrate in reaction chamber, introducing 10-1000 sccm protective gas and keeping for 1-60 minutes in reaction chamber, heating to 750-1100 degrees C, introducing gaseous carbon-containing material at flow rate of 20-1000 sccm and gaseous nitrogen-containing material at flow rate of 10-200sccm with atomic ratio carbon:nitrogen of 2-20:1, and maintaining reaction for 1-300 minutes to obtain product on surface of substrate. USE - Preparation of doped graphene (claimed). ADVANTAGE - Doped graphene has low oxygen content and uniform nitrogen content, and preparation process is simple, does not need catalyst, and has simple operation and device. DESCRIPTION OF DRAWING(S) - The drawing shows XPS spectrum of nitrogen-doped graphite.