• 专利标题:   Preparation of composite building material involves modifying prepared oxidized graphite, preparing MC nylon/modified graphene nanocomposite using modified product, adding e.g. accelerant and polyisocyanate trimer, and sintering.
  • 专利号:   CN106243701-A
  • 发明人:   YANG D
  • 专利权人:   SUZHOU RUITEJIE CHEM PROD CO LTD
  • 国际专利分类:   C08G069/14, C08G069/16, C08K013/06, C08K003/04, C08K003/22, C08K003/34, C08K005/5313, C08K009/04, C08L027/18, C08L061/06, C08L077/02, C08L009/02
  • 专利详细信息:   CN106243701-A 21 Dec 2016 C08L-077/02 201725 Pages: 6 Chinese
  • 申请详细信息:   CN106243701-A CN10617577 01 Aug 2016
  • 优先权号:   CN10617577

▎ 摘  要

NOVELTY - Preparation of composite building material involves preparing oxidized graphite with high oxidation degree, modifying with cetyltrimethylammonium bromide, preparing a MC nylon/modified graphene nanocomposite by in-situ polymerization using the resultant modified product, adding e.g. a nitrile rubber modified phenolic resin, methenamine, hexamethylenetetramine, amyl triethoxysilane, conductive mica powder, polyisocyanate trimer, polytetrafluoroethylene fibers, a nano active agent, a plasticizer, nano cerium oxide and an accelerant, mixing, extruding, sintering, and cooling. USE - Preparation of composite building material (claimed). ADVANTAGE - The method enables preparation of environmentally-friendly composite building material having excellent flame retardance, high-temperature resistance, mechanical property, comprehensive performance and low-expansion performance, by effective adsorption and removal of harmful gases and dust in exhaust gas. The molten resin used in preparation of the building material is rapidly transformed from linear structure into non-molten structure. DETAILED DESCRIPTION - Preparation of composite building material involves preparing oxidized graphite with high oxidation degree, modifying with cetyltrimethylammonium bromide, preparing a MC nylon/modified graphene nanocomposite by in-situ polymerization using the resultant modified product, adding a nitrile rubber modified phenolic resin, methenamine, a vacuum residue, a non-halogenated organic phosphinate, hexamethylenetetramine, amyl triethoxysilane, conductive mica powder, conductive nano-graphite powder, polyisocyanate trimer, polytetrafluoroethylene fibers, a nano active agent, a plasticizer, an antioxidant, nano cerium oxide and an accelerant, crushing, mixing, screening by 100-200 mesh sieve, stirring at 90-100 degrees C, obtaining a base material, extruding in a vacuum extruder at vacuum degree of 1-1.8 MPa and extrusion pressure of 15-20 MPa, drying, sintering at 700 degrees C for 15 days, placing obtained product in a casting machine, pressurizing, melting at 160-190 degrees C, heat-preserving for 3-5 hours, and naturally cooling. The composite building material contains 8-10 pts. wt. nitrile rubber modified phenolic resin, 15-20 pts. wt. methenamine, 5-10 pts. wt. vacuum residue, 5-7 pts. wt. non-halogenated organic phosphinate, 8-10 pts. wt. hexamethylenetetramine, 2-4 pts. wt. amyl triethoxysilane, 0.3-0.5 pt. wt. conductive mica powder, 0.2-0.4 pt. wt. conductive nano-graphite powder, 0.8-1 pt. wt. polyisocyanate trimer, 1-2 pts. wt. polytetrafluoroethylene fibers, 20-30 pts. wt. nano active agent, 2-8 pts. wt. plasticizer, 1-5 pts. wt. antioxidant, 6-14 pts. wt. nano cerium oxide and 2-6 pts. wt. accelerant.