• 专利标题:   Preparing super network structure graphene oxide gel useful for adsorbing heavy metal ions or dye comprises e.g. providing under the aid of ultrasound, dispersing oxidized graphene uniformly.
  • 专利号:   CN106749923-A, CN106749923-B
  • 发明人:   HAN J, ZHANG Y, LIU F
  • 专利权人:   UNIV QINGDAO SCI TECHNOLOGY, UNIV QINGDAO SCI TECHNOLOGY
  • 国际专利分类:   C01B032/198, C08F002/44, C08F002/56, C08F220/56, C08F251/00, C08J003/075, C08K003/04
  • 专利详细信息:   CN106749923-A 31 May 2017 C08F-251/00 201747 Pages: 9 Chinese
  • 申请详细信息:   CN106749923-A CN11149170 14 Dec 2016
  • 优先权号:   CN11149170

▎ 摘  要

NOVELTY - Preparing super network structure graphene oxide gel comprises e.g. providing under the aid of ultrasound, dispersing 1 pts. wt. oxidized graphene uniformly, where three-necked flask containing 100 pts. wt. deionized water, dispersing evenly after the transfer to the magnetic stirrer, adding 0.1-1.5 pts. wt. glacial acetic acid, stirring evenly, adding 0.1-3 pts. wt. polyglucosamine (1-4) -2-amino-B-D powder, stirring to prepare a polyglucosamine (1-4) -2-amino-B-D acetic acid solution, synthesizing graphene oxide using an improved hummers method, and providing ice water bath. USE - The gel is useful for adsorbing heavy metal ions or dye (claimed). ADVANTAGE - The method: does not use initiator; is carried out at low temperature and fast reaction speed; is economical; environmentally friendly; and easy realization of industrialization. DETAILED DESCRIPTION - Preparing super network structure graphene oxide gel comprises (i) providing under the aid of ultrasound, dispersing 1 pts. wt. oxidized graphene uniformly, where three-necked flask containing 100 pts. wt. deionized water, dispersing evenly after the transfer to the magnetic stirrer, adding 0.1-1.5 pts. wt. glacial acetic acid, stirring evenly, adding 0.1-3 pts. wt. polyglucosamine(1-4)-2-amino-B-D powder, stirring until completely dissolved to prepare a polyglucosamine(1-4)-2-amino-B-D acetic acid solution, synthesizing graphene oxide using an improved hummers method, providing ice water bath, resulting polyglucosamine(1-4)-2-amino-B-D acetic acid solution add certain amount of acrylamide monomer and an active agent sequentially, stirring evenly at a certain intensity of ultrasound through inert gas, ultrasound sterilizing for 10-60 minutes, transferring the solution to a polytetrafluoroethylene mold at 50-60 degrees C, water bath reacting for 4-10 hours, and obtaining super network structure oxide graphene oxide gel. An INDEPENDENT CLAIM is also included for super network structure graphene oxide oxide gel.