• 专利标题:   Preparing high strength and high conductivity graphene reinforced copper matrix composite material useful for e.g. automobile, aerospace and electronic field, comprises mixing graphene with absolute ethanol, ball milling, heating and drying.
  • 专利号:   CN108145169-A
  • 发明人:   WANG D, WANG P, FENG Y
  • 专利权人:   NO 725 RES INST CHINA SHIPBUILDING IND C
  • 国际专利分类:   B22F009/04, B22F001/00, B22F001/02, B22F003/04, B22F003/15, B22F003/20, C22C001/05, C22C009/00
  • 专利详细信息:   CN108145169-A 12 Jun 2018 B22F-009/04 201849 Pages: 10 Chinese
  • 申请详细信息:   CN108145169-A CN11201425 27 Nov 2017
  • 优先权号:   CN11201425

▎ 摘  要

NOVELTY - Preparing high strength and high conductivity graphene reinforced copper matrix composite material comprises mixing graphene with absolute ethanol, carrying out high-speed shear dispersion treatment and ultrasonically vibration treatment to obtain monodisperse of graphene, mixing graphene monodispersant with copper powder, carrying out ball milling pre-dispersion to obtain a mixture of graphene/copper composite powder and ethanol, taking the obtained mixture of the graphene/copper composite powder and ethanol, heating, drying to obtain graphene copper composite, coating the obtained graphene copper composite to obtain a graphene copper composite, taking the obtained hydrogen reduction treatment of the graphene copper composite of the core-shell structure, to obtain graphene copper powder, subjecting the graphene copper powder obtained for cold isostatic pressing to obtain a cold pressed billet, welding and sealing, subjecting to hot isostatic pressing treatment, hot extrusion molding. USE - The high strength and high conductivity graphene reinforced copper matrix composite material is useful for automobile, aerospace and electronic field (claimed). ADVANTAGE - The material has high bonding with substrate interface and stable performance. DETAILED DESCRIPTION - Preparing high strength and high conductivity graphene reinforced copper matrix composite material comprises (a) mixing graphene with absolute ethanol, carrying out high-speed shear dispersion treatment and ultrasonically vibration treatment to obtain monodisperse of graphene, evenly mixing the graphene monodispersant with the copper powder, carrying out ball milling pre-dispersion to obtain a mixture of graphene/copper composite powder and ethanol, (b) under stirring conditions, taking the obtained mixture of the graphene/copper composite powder and the ethanol, heating to a viscous liquid bath, drying to obtain graphene copper composite, (c) coating the obtained graphene copper composite to obtain a graphene copper composite having a core-shell structure, (d) taking the obtained hydrogen reduction treatment of the graphene copper composite of the core-shell structure, reducing the oxygen contained in the composite to obtain graphene copper powder, (e) subjecting the graphene copper powder obtained for cold isostatic pressing to obtain a cold pressed billet, (f) after the cold-pressed ingot obtained, welding, under heating conditions, vacuuming the jacket, when the degree of vacuum is less than 1x 10-3Pa, welding and sealing, (g) welding and sealing the jacket, subjecting to hot isostatic pressing treatment to obtain a graphene-reinforced copper matrix composite material, and (h) hot extrusion molding of graphene-reinforced copper matrix composite material to obtain high-strength, high-conductivity graphene-reinforced copper-based composite material. An INDEPENDENT CLAIM is also included for high strength and high conductivity graphene reinforced copper matrix composite material is obtained by above method.