• 专利标题:   Immersion method for preparing graphene/copper composite material, involves preparing flaky copper powder particles, immersing copper powder in poly(methyl methacrylate) solution, filtering and thermally reducing PMMA-copper powder.
  • 专利号:   CN105081312-A, CN105081312-B
  • 发明人:   HE C, LIU E, SHI C, ZHAO N, CHEN Y
  • 专利权人:   UNIV TIANJIN
  • 国际专利分类:   B22F001/02, C01B031/04, C01B032/184
  • 专利详细信息:   CN105081312-A 25 Nov 2015 B22F-001/02 201632 Pages: 9 English
  • 申请详细信息:   CN105081312-A CN10506051 17 Aug 2015
  • 优先权号:   CN10506051

▎ 摘  要

NOVELTY - Immersion method for preparing graphene/copper composite material, where solid carbon source is loaded on copper surface, involves preparing flaky copper powder particles by adding atomized copper powder and steel balls to a ball mill jar, filling alcohol for wet grinding, and vacuum drying, dissolving poly(methyl methacrylate)(PMMA) in dimethylformamide or acetone solution, immersing sheet-like copper powder in the mixed solution, carrying out hydrothermal or suction filtration, drying, and thermally reducing PMMA-copper powder in reduction tube furnace. USE - Immersion method for preparing graphene/copper composite material, where solid carbon source is loaded on copper surface (claimed). ADVANTAGE - The method ensures preparation of graphene/copper composite materials with different matrix by simple process. DETAILED DESCRIPTION - Immersion method for preparing graphene/copper composite material, where solid carbon source is loaded on copper surface, involves preparing flaky copper powder particles by adding atomized copper powder and steel balls in mass ratio of 1:15 to a ball mill jar, filling alcohol for wet grinding for 4 hours, and vacuum drying, dissolving poly(methyl methacrylate) (PMMA) in dimethylformamide or acetone solution, immersing sheet-like copper powder in the mixed solution, stirring for 6 hours, evaporating to dryness, carrying out hydrothermal reaction or suction filtration and drying to obtain a uniform loaded PMMA/copper composite powder, carrying out thermal reduction of PMMA/copper composite material by loading PMMA-copper powder into reduction tube furnace, and maintaining at a temperature of 1000 degrees C under reducing atmosphere of hydrogen.