• 专利标题:   Treating high fluorine content of domestic water involves taking graphene oxide, then adding with silver nitrate, and mixing under ultrasonication to obtain mixture and adding with sodium hydroxide solution under magnetic stirring.
  • 专利号:   CN107413294-A
  • 发明人:   LIN C, XUE D, LIU S
  • 专利权人:   UNIV XIAN SHIYOU
  • 国际专利分类:   B01J020/20, C02F001/28, C02F001/50, C02F101/14
  • 专利详细信息:   CN107413294-A 01 Dec 2017 B01J-020/20 201801 Pages: 7 Chinese
  • 申请详细信息:   CN107413294-A CN10358474 19 May 2017
  • 优先权号:   CN10358474

▎ 摘  要

NOVELTY - Treating high fluorine content of domestic water involves taking 20-30ml 2-6mmol/L graphene oxide, then adding with 3-5ml 10 mmol/L silver nitrate, and mixing under ultrasonication for 30 minutes to obtain mixture. The mixture is drop-wise added with 7 mol/L sodium hydroxide solution under magnetic stirring, then cooling, filtering and washing with water. The mixture is then drop-wise added with 0.05 M 3-5ml silver nitrate under stirring with the addition of 2 wt.% aqueous ammonia without precipitation, and 37 wt.% 1ml formaldehyde and incubating for 2 hours to obtain reaction product. USE - Method for treat high fluorine content of domestic water (claimed). ADVANTAGE - The method enables to treat high fluorine content of domestic water, which is non-toxic to human body, is eco-friendly and prepared in a simple, safe and energy-saving manner. DETAILED DESCRIPTION - Treating high fluorine content of domestic water involves taking 20-30ml 2-6mmol/L graphene oxide, then adding with 3-5ml 10 mmol/L silver nitrate, and mixing under ultrasonication for 30 minutes to obtain mixture. The mixture is drop-wise added with 7 mol/L sodium hydroxide solution under magnetic stirring, then cooling, filtering and washing with water. The mixture is then drop-wise added with 0.05 M 3-5ml silver nitrate under stirring with the addition of 2 wt.% aqueous ammonia without precipitation, and 37 wt.% 1ml formaldehyde and incubating for 2 hours to obtain reaction product. The reaction product is poured into a centrifuge tube, then centrifuged under stirring speed of 8000 revolutions/minute for 5 minutes, then separated by incubating, and washed with water and alcohol for three times, and drying in oven at 80 degrees C for 3 hours to obtain desired product.