• 专利标题:   Composite photocatalyst bismuth vanadate loaded with iron-doped tungstic oxide modified graphene, for photolysis of water, involves dispersing sea-urchin-shaped nano iron-doped tungstic oxide and flower-shaped bismuth vanadate loaded graphene in deionized water, vacuum drying, and calcining.
  • 专利号:   CN113398915-A
  • 发明人:   WU Y
  • 专利权人:   HANGZHOU HUIXIA NEW MATERIAL CO LTD
  • 国际专利分类:   B01J023/22, B01J023/888, B01J035/00, B01J035/02, C01B003/04
  • 专利详细信息:   CN113398915-A 17 Sep 2021 B01J-023/22 202191 Pages: 6 Chinese
  • 申请详细信息:   CN113398915-A CN10562755 24 May 2021
  • 优先权号:   CN10562755

▎ 摘  要

NOVELTY - A composite photocatalyst bismuth vanadate loaded with iron-doped tungstic oxide modified graphene, involves adding sodium tungstate and ferric nitrate to hydrochloric acid solution with a pH of 1.5-2, stirring and dissolving, adding isopropanol, pouring the solution into a crystallization reactor, filtering the solvent, washing the product with deionized water to neutral, and calcining in a muffle furnace to obtain a sea-urchin-shaped nano iron-doped tungstic oxide, adding bismuth nitrate, ammonium metavanadate, and graphene quantum dots to deionized water, ultrasonically dispersing, adjusting the pH to 3-4, pouring the solution into a crystallization reactor, filtering the solvent, and washing the product with deionized water to obtain flower-shaped bismuth vanadate loaded graphene, adding the nano iron-doped tungstic oxide and bismuth vanadate loaded graphene to deionized water, ultrasonically dispersing, vacuum drying, and calcining in a muffle furnace. USE - Composite photocatalyst bismuth vanadate loaded with iron-doped tungstic oxide modified graphene, is used for photolysis of water. ADVANTAGE - The composite photocatalyst effectively separates the photogenerated carrier, avoiding recombination, to generate a large amount of photo-generated electrons and holes, and reduces water to generate hydrogen and oxidizes to generate oxygen.