• 专利标题:   Graphene material in the fields of textiles, coatings and plastics, is having a fiber shape, and prepared by subjecting cellulose raw material to acid treatment to separate cellulose and hemicellulose, and collecting solid.
  • 专利号:   CN111270350-A
  • 发明人:   DU Q, LONG S, TANG P, HUANG R
  • 专利权人:   GUANGXI ACAD SCI
  • 国际专利分类:   C01B032/184, D01F009/16
  • 专利详细信息:   CN111270350-A 12 Jun 2020 D01F-009/16 202056 Pages: 12 Chinese
  • 申请详细信息:   CN111270350-A CN10097892 31 Jan 2019
  • 优先权号:   CN10097892

▎ 摘  要

NOVELTY - Graphene material is having a fiber shape, where the diameter of the graphene material is 10 nanometer-20 micrometer, and length of the graphene material is 100 micrometer. USE - Graphene material used in the fields of textiles, coatings and plastics (claimed). ADVANTAGE - The graphene material expands the application range of the graphene material. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for a method for preparing a graphene material, which involves: (A) subjecting cellulose raw material to acid treatment to separate cellulose and hemicellulose, collecting solid to obtain a crude crude cellulose extract; (B) subjecting first crude cellulose extract obtained is subjected to alkali treatment to separate cellulose and lignin in the crude cellulose extract, and collecting solid to obtain a second crude cellulose extract; (C) heat-treating cellulose secondary crude extract and formic acid to further remove hemicellulose and lignin, and collecting solids to obtain a pure cellulose product, where the diameter of the pure cellulose product is 10 micrometer-20 micrometer; (D) subjecting pure cellulose product obtained to temperature-programming treatment in an inert gas environment to obtain a cellulose carbonized product; and (E) cooling graphitized cellulose carbonized product after being graphitized to obtain a graphene material having a fiber shape.