• 专利标题:   Growing large-domain graphene by using hexagonal boron nitride as a seed involves providing substrate, dissolving hexagonal boron nitride in solvent, and then stirring obtained mixture ultrasonically treating the boron nitride particles.
  • 专利号:   CN107244666-A
  • 发明人:   YU F, ZHANG J, YANG Z, SUN L, LI Y, CHENG X, ZHAO X
  • 专利权人:   UNIV SHANDONG
  • 国际专利分类:   C01B032/188
  • 专利详细信息:   CN107244666-A 13 Oct 2017 C01B-032/188 201779 Pages: 12 Chinese
  • 申请详细信息:   CN107244666-A CN10399638 31 May 2017
  • 优先权号:   CN10399638

▎ 摘  要

NOVELTY - Growing large-domain graphene by using hexagonal boron nitride as a seed involves providing substrate. The hexagonal boron nitride is dissolved in the solvent. The obtained mixture is stirred ultrasonically treating the boron nitride particles uniformly dispersed. The obtained mixture is kept stand. The hexagonal boron nitride solution is sprayed onto the surface of the substrate to obtain substrate coated with hexagonal boron nitride. The coated substrate of hexagonal boron nitride is kept in a chemical vapor deposition tubular furnace. USE - Method for growing large-domain graphene by using hexagonal boron nitride as a seed (claimed). ADVANTAGE - The method enables to grow large-domain graphene by using hexagonal boron nitride as a seed with improved quality of graphene growth. DETAILED DESCRIPTION - Growing large-domain graphene by using hexagonal boron nitride as a seed involves providing substrate. The hexagonal boron nitride is dissolved in the solvent. The obtained mixture is stirred ultrasonically treating the boron nitride particles uniformly dispersed. The obtained mixture is kept stand. The hexagonal boron nitride solution is sprayed onto the surface of the substrate to obtain substrate coated with hexagonal boron nitride. The coated substrate of hexagonal boron nitride is kept in a chemical vapor deposition tubular furnace. The obtained product is vacuumized and heated after filling high pure argon and hydrogen. The temperature of the obtained product is raised at 950-1200 degrees C to carry out hydrogen etching. The carbon source gas after hydrogen etching is introduced. The insulating nitride is central to grow graphene. The obtained product is cooled at 600-700 degrees C under the inert atmosphere.