• 专利标题:   Preparing regenerated bacterial cellulose composite aerogel adsorption material useful e.g. in absorbing dye comprises adding bacterial cellulose powder to mixed solution e.g. urea, pre-cooling, adding e.g. attapulgite and freeze-drying.
  • 专利号:   CN113083249-A
  • 发明人:   ZHANG J, SONG S, JIAO C, LIU X, DING L, HUANG Y, YANG S, FAN Z
  • 专利权人:   UNIV NORTHWEST NORMAL
  • 国际专利分类:   B01J020/26, B01J020/28, B01J020/30, C02F001/28, C02F101/20, C02F101/30
  • 专利详细信息:   CN113083249-A 09 Jul 2021 B01J-020/26 202163 Pages: 11 Chinese
  • 申请详细信息:   CN113083249-A CN10261747 10 Mar 2021
  • 优先权号:   CN10261747

▎ 摘  要

NOVELTY - Preparing regenerated bacterial cellulose composite aerogel adsorption material comprises (a) adding the bacterial cellulose powder to the mixed solution of sodium hydroxide, urea and water, pre-cooling at -12 to-20 degrees C for 30-60 minutes, stirring for 10-30 minutes to obtain a transparent bacterial cellulose solution and (b) adding the polyvinyl alcohol into the bacterial cellulose solution, stirring, dissolving, adding graphene oxide and attapulgite, dispersing uniformly, ultrasonically removing bubbles, casting the mixed solution into 12-hole culture plate, freezing and thawing to form columnar composite hydrogel, washing the hydrogel with distilled water to pH of 7.0 and freeze-drying to obtain the regenerated bacterial cellulose composite aerogel adsorption material bacterial cellulose / polyvinyl alcohol / graphene oxide/attapulgite. USE - The regenerated bacterial cellulose composite aerogel adsorption material is useful in absorbing dye and absorbing heavy metal ions, preferably copper ions and lead ions (claimed). ADVANTAGE - The adsorption material has low preparation cost, good acid-base stability and thermal stability, has good adsorption capacity for Congo red, methylene blue dyes and copper ions and lead ions heavy metal ions; has high regeneration rate after repeated use and used in industrial wastewater purification treatment.