• 专利标题:   Preparation of graphene/magnesium nanoparticle composite material involves adding graphene oxide, dissolving magnesium chloride, adjusting pH value, ultrasonically stirring, transferring into reaction kettle, reacting, cooling, and mixing.
  • 专利号:   CN107297512-A, CN107297512-B
  • 发明人:   WANG Y
  • 专利权人:   NANLING PRODUCTIVITY PROMOTION CENT
  • 国际专利分类:   B22F001/00, B22F009/24, B82Y030/00, B82Y040/00, C01B032/184
  • 专利详细信息:   CN107297512-A 27 Oct 2017 B22F-009/24 201779 Pages: 6 Chinese
  • 申请详细信息:   CN107297512-A CN10516108 29 Jun 2017
  • 优先权号:   CN10516108

▎ 摘  要

NOVELTY - Preparation of graphene/magnesium nanoparticle composite material involves adding 1.5 mg/L graphene oxide, dissolving 450 mu mol/L magnesium chloride in 0.2 mol/L phosphoric acid buffer salt solution, adjusting pH value to 10, and ultrasonically stirring for 20 minutes to obtain uniform suspension; transferring suspension into reaction kettle, reacting for 12 hours at 100-120 degrees C, cooling to room temperature, taking out, and washing by deionized water to obtain precipitate; and putting precipitate in tube-type resistance furnace for heat treatment, and mixing argon-hydrogen gas. USE - Method for preparing graphene/magnesium nanoparticle composite material (claimed). ADVANTAGE - The method has cheap price, and wide application. DETAILED DESCRIPTION - Preparation of graphene/magnesium nanoparticle composite material comprises adding 1.5 mg/L graphene oxide, dissolving 450 mu mol/L magnesium chloride in 0.2 mol/L phosphoric acid buffer salt solution, adjusting pH value to 10, and ultrasonically stirring for 20 minutes to obtain uniform suspension; transferring suspension into reaction kettle, reacting for 12 hours at 100-120 degrees C, cooling to room temperature, taking out, and washing by deionized water to obtain precipitate; and putting precipitate in tube-type resistance furnace for heat treatment, mixing argon-hydrogen gas, raising temperature to 600-700 degrees C, preserving heat for 3 hours, closing heating power supply, and naturally cooling to room temperature.