• 专利标题:   Preparation of graphene by heating expandable graphite under protective gas atmosphere, thermally peeling, dissolving in surfactant solution, performing ultrasonic peeling, centrifuging, filtering, washing, drying and heating via microwave.
  • 专利号:   CN102464315-A
  • 发明人:   ZHOU M, WU F, WANG Y
  • 专利权人:   HAIYANGWANG LIGHTING TECHNOLOGY CO LTD, OCEANS KING LIGHTING SCI TECHNOLOGY CO
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN102464315-A 23 May 2012 C01B-031/04 201317 Pages: 8 Chinese
  • 申请详细信息:   CN102464315-A CN10548936 18 Nov 2010
  • 优先权号:   CN10548936

▎ 摘  要

NOVELTY - Graphene is prepared by (1) heating expandable graphite under protective gas atmosphere, performing thermal peeling to obtain expanded graphite; (2) dissolving the expanded graphite in surfactant solution (A) to obtain a mixture (B), subjecting the mixture (B) into ultrasonic peeling to obtain graphene solution (C); (3) centrifuging, filtering, washing and drying the graphene solution (C) to obtain graphene crude product; and (4) heating the graphene crude product via microwave to obtain graphene. USE - Method for preparing graphene (claimed). ADVANTAGE - The method is simple and convenient to operate, and can provide graphene with high purity, low cost and high yield, thus making it suitable for large-scale production.