• 专利标题:   Preparation of graphene-based protective fabric involves dissolving graphene oxide in N,N-dimethylformamide, heating, adding hydrazine hydrate reduction reaction, washing, pelletizing, intertwinning, and connecting.
  • 专利号:   CN111235676-A, CN111235676-B
  • 发明人:   CHEN C
  • 专利权人:   CHEN C, NINGBO SNOWWOLF OUTDOOR APPAREL CO LTD
  • 国际专利分类:   D01F001/10, D01F006/92
  • 专利详细信息:   CN111235676-A 05 Jun 2020 D01F-006/92 202054 Pages: 10 Chinese
  • 申请详细信息:   CN111235676-A CN10198434 19 Mar 2020
  • 优先权号:   CN10198434

▎ 摘  要

NOVELTY - Preparation of graphene-based protective fabric involves dissolving graphene oxide in N,N-dimethylformamide, heating up to 80-90 degrees C, adding diisocyanate with preset mass ratio, reacting for 2-4 hours, heating up to 90-100 degrees C, adding hydrazine hydrate reduction reaction for 1-4 hours, centrifuging, washing to obtain modified graphene, adding hydroxyl-terminated polyester to reaction vessel, raising temperature to 275-285 degrees C to melting, adding obtained modified graphene to melted hydroxyl-terminated in polyester, stirring, reacting for 2-4 hours, cooling, pelletizing to obtain modified polyester masterbatch, melt-spinning obtained modified polyester masterbatch to obtain modified polyester fiber, crossing obtained modified polyester fiber, intertwinning, and connecting. USE - Preparation of graphene-based protective fabric. ADVANTAGE - The method has improved load fastness of graphene on fabric through chemical bonding. The fabric has improved protection durability of fabric against pneumonia bacteria.