• 专利标题:   Production of carbon nanotubes for preparing graphene nanoribbons, involves subjecting metal substrate to acid treatment, heating substrate, ultrasonically-treating, and processing substrate in chemical vapor deposition reactor.
  • 专利号:   CN103933976-A
  • 发明人:   YAN C, YI W
  • 专利权人:   YI W
  • 国际专利分类:   B01J023/644
  • 专利详细信息:   CN103933976-A 23 Jul 2014 B01J-023/644 201468 Pages: 13 Chinese
  • 申请详细信息:   CN103933976-A CN10191596 08 May 2014
  • 优先权号:   CN10191596

▎ 摘  要

NOVELTY - Production of carbon nanotubes involves subjecting a metal substrate to acid treatment in an oxygen-free environment, heating substrate at 600-900 degrees C, ultrasonically-treating, placing substrate in chemical vapor deposition reactor containing gaseous carbonaceous material, supplying protective gas to the reactor and removing carbon nanotubes from the substrate. USE - Production of carbon nanotubes used for preparing graphene nanoribbons (all claimed). ADVANTAGE - The method efficiently and economically provides carbon nanotubes with high thickness and shape uniformity using simple process under controlled reaction conditions. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are included for the following: (1) carbon nanotubes; (2) preparation of graphene nanoribbons, which involves mixing carbon nanotubes and metal chloride in mass ratio of 1:0.8-1:1.2 at 460-550 degrees C and obtaining metal chloride-intercalated carbon nanotubes, mixing metal chloride-intercalated carbon nanotubes and acetone in mass ratio of 1 g:100-1000 mL, ultrasonically peeling after separation and purifying; and (3) graphene nanoribbons.