• 专利标题:   Making freeze-dried sponge-like graphene, by adding natural graphite and ultrasonically concentrated sulfuric acid in ice bath, mixing sodium nitrate and potassium permanganate, adding water and hydrogen peroxide solution and freeze-drying.
  • 专利号:   CN104163423-A
  • 发明人:   WANG H, YU X, WU X
  • 专利权人:   UNIV DONGHUA
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN104163423-A 26 Nov 2014 C01B-031/04 201507 Pages: 8 Chinese
  • 申请详细信息:   CN104163423-A CN10397019 13 Aug 2014
  • 优先权号:   CN10397019

▎ 摘  要

NOVELTY - Making freeze-dried sponge-like graphene, comprises adding natural graphite and ultrasonically concentrated sulfuric acid in an ice bath and mixing for 15-60 minutes, adding sodium nitrate and potassium permanganate and mixing for 15-60 minutes, reacting the mixture for 0.5 hours, placing the mixed liquid in a water bath and stirring at 30-35 degrees C for 0.5-1.5 hours, adding deionized water to the mixed liquid, heating at 95-10 degrees C and stirring for 20-30 minutes, adding deionized water and hydrogen peroxide solution, centrifuging, washing, freeze-drying and heating at low pressure. USE - The method is useful for making freeze-dried sponge-like graphene (claimed). ADVANTAGE - The method rapidly, efficiently, simply and easily makes the freeze-dried sponge-like graphene with reduced energy consumption in an eco-friendly manner.