• 专利标题:   Preparation of silica-based nano-multilayer hollow capsule one-dimensional photonic crystal film involves preparing nano-silica multilayer hollow capsules, fixing on silicon, and applying titania and graphene oxide colloidal solution.
  • 专利号:   CN103896627-A, CN103896627-B
  • 发明人:   GE L, YAO C, ZHU Y, REN J
  • 专利权人:   UNIV SOUTHEAST
  • 国际专利分类:   C04B041/85, C04B041/89
  • 专利详细信息:   CN103896627-A 02 Jul 2014 C04B-041/85 201460 Pages: 9 Chinese
  • 申请详细信息:   CN103896627-A CN10073201 28 Feb 2014
  • 优先权号:   CN10073201

▎ 摘  要

NOVELTY - Preparation of silica-based nano-multilayer hollow capsule one-dimensional photonic crystal film involves preparing self-assembled layers of nano-silica multilayer hollow capsules, washing silicon substrate, fixing nano-silica layer hollow capsules on silicon surface by performing spin-coating, obtaining one-dimensional photonic crystal substrate film, preparing titania colloidal solution and graphene oxide colloidal solution, performing layer by layer by a spin coating, and applying titania colloidal solution and graphene oxide colloidal solution into bottom surface of substrate. USE - Preparation of silica-based nano-multilayer hollow capsule one-dimensional photonic crystal film (claimed). ADVANTAGE - The silica-based nano-multilayer hollow capsule one-dimensional photonic crystal film has high sensitivity of detection, and is prepared by simple, effective and easy method within short period of time. DETAILED DESCRIPTION - Preparation of silica-based nano-multilayer hollow capsule one-dimensional photonic crystal film involves preparing self-assembled layers of nano-silica multilayer hollow capsules, washing silicon substrate, drying, fixing nano-silica layer hollow capsules on silicon surface by performing spin-coating with speed of 3000-6000 rpm for 30 seconds to 1 minute, obtaining one-dimensional photonic crystal substrate film, preparing titania colloidal solution having concentration of 7.8-39 mg/ml and graphene oxide colloidal solution having concentration of 0.1-0.5 mg/ml, performing layer by layer by a spin coating with speed of 3000-6000 rpm for 30 seconds to 1 minute, applying titania colloidal solution and graphene oxide colloidal solution into bottom surface of substrate, obtaining silica-based nano-multilayer hollow capsule one-dimensional photonic crystal film.