• 专利标题:   Thermal insulating coating comprises acrylic resin, butyronitrile rubber 2707, phenolic resin, N,N'-xylyl-phenylene diamine, modified graphene, talcum powder, calcined kaolin, hollow microsphere and 3-glycidoxypropyltrimethoxysilane.
  • 专利号:   CN104312335-A, CN104312335-B
  • 发明人:   MA C, CAO Y, ZHANG X
  • 专利权人:   QIAOJIAN NEW ENERGY TECHNOLOGY SUZHOU CO, GUANGZHOU ZHEMING INK PAINT CO LTD
  • 国际专利分类:   C09D109/02, C09D133/00, C09D161/06, C09D007/12
  • 专利详细信息:   CN104312335-A 28 Jan 2015 C09D-133/00 201523 Pages: 6 Chinese
  • 申请详细信息:   CN104312335-A CN10611928 04 Nov 2014
  • 优先权号:   CN10611928

▎ 摘  要

NOVELTY - Thermal insulating coating comprises e.g. 50-55 pts. wt. acrylic resin, 22-26 pts. wt. butyronitrile rubber 2707, 18-21 pts. wt. phenolic resin, 1.1-1.4 pts. wt. N,N'-xylyl-phenylene diamine as antiaging agent 4010NA, 23-26 pts. wt. modified graphene, 10-13 pts. wt. talcum powder, 8-11 pts. wt. calcined kaolin, 3-6 pts. wt. hollow microsphere, 1.1-1.5 pts. wt. 3-glycidoxypropyltrimethoxysilane as silane coupling agent KH-560, 1.4-1.8 pts. wt. coalescing aids, 2.2-2.5 pts. wt. dispersing agent, 1.6-1.9 pts. wt. defoaming agent and 1-1.5 pts. wt. thickening agent. USE - Thermal insulating coating. ADVANTAGE - The thermal insulating coating has high adhesive force and good shock resistance. DETAILED DESCRIPTION - Thermal insulating coating comprises 50-55 pts. wt. acrylic resin, 22-26 pts. wt. butyronitrile rubber 2707, 18-21 pts. wt. phenolic resin, 1.1-1.4 pts. wt. N,N'-xylyl-phenylene diamine as antiaging agent 4010NA, 23-26 pts. wt. modified graphene, 10-13 pts. wt. talcum powder, 8-11 pts. wt. calcined kaolin, 3-6 pts. wt. hollow microsphere, 1.1-1.5 pts. wt. 3-glycidoxypropyltrimethoxysilane as silane coupling agent KH-560, 1.4-1.8 pts. wt. coalescing aids, 2.2-2.5 pts. wt. dispersing agent, 1.6-1.9 pts. wt. defoaming agent, 1-1.5 pts. wt. thickening agent, 1.8-2.1 pts. wt. wetting agent, 1.6-2 pts. wt. flatting agent, 0.3-0.6 pts. wt. preservative, 0.2-0.5 pts. wt. mildew preventive agent and 58-62 pts. wt. solvent. The modified graphene is prepared by adding 3-6 pts. wt. graphene, 8-10 pts. wt. sodium nitrite at a concentration of 1.2-1.5 mmole/l and 15-18 pts. wt. n-hexyl alcohol into a first reaction vessel, stirring the reaction vessel at a stirring speed of 110-115 revolutions per minute for 0.6-1 hour, adding 0.5-0.8 pts. wt. sulfuric acid solution, heating the first reaction vessel at 66-70 degrees C under stirring speed of 90-110 revolutions per minute for 1.2-1.8 hours, cooling to 25-28 degrees C, then drying the obtained material (A), centrifugally separating the dried material at a speed of 3600-3800 revolutions per minute, adding the material A, 4-7 pts. wt. acetone, 6-9 pts. wt. vitamin C, and 3-5 pts. wt. nitroaniline into a second reaction container, standing the reaction mixture for 16-18 hours, ultrasonically dispersing the reaction mixture at frequency of 36-40 KHZ and ultrasonic dispersion power of 950-1100 W for 1-3 hours, filtering and drying a modified graphene.