• 专利标题:   Producing oxidized graphene flakes by reacting sulfuric acid or mixture of orthophosphoric acid and sulfuric acid with graphite powder, cooling, adding oxidant, heating, supplying deionized water, and stopping reaction with perhydrol.
  • 专利号:   PL430819-A1
  • 发明人:   KACZMAREK L, MAKOWICZ M, WARGA T, STEGLINSKI M, ZAKRZEWSKI S, BATORY D, PELKA M, KUTEN D, NAZIM T, GALAZKA M
  • 专利权人:   ADVANCED GRAPHENE PROD SP ZOO
  • 国际专利分类:   B82Y040/00, C01B032/198
  • 专利详细信息:   PL430819-A1 08 Feb 2021 C01B-032/198 202154 Pages: 1
  • 申请详细信息:   PL430819-A1 PL430819 06 Aug 2019
  • 优先权号:   PL430819

▎ 摘  要

NOVELTY - Oxidized graphene flakes are produced by adding sulfuric acid or mixture of orthophosphoric acid and sulfuric acid to graphite powder introduced into a reaction chamber of a reactor, setting pressure and temperature to 1-200 bar and 50-200 degrees C, respectively, mixing introduced components using magnetic stirrer or acoustic or ultrasonic homogenizer, and after 1-4 hours, cooling resulting reaction mixture to 0 degrees C, introducing 40-95 mass% oxidant into reaction chamber with continuous stirring, heating enriched mixture to 30-55 degrees C for 2-6 hours, with continuous mixing under pressure of 1-200 bar, after 1-24 hours, supplying deionized water to reaction chamber in an amount corresponding to a volume ratio of 1:2-3:1 with respect to acids, stopping reaction by adding perhydrol in a volume ratio of 1:20, based on the volume of the mixture, and removing finished product from reaction chamber of reactor via discharge valve. USE - Production of oxidized graphene flakes.