• 专利标题:   Preparing conductive, wave-absorbing and anti-corrosion integrated coating based on two-dimentional carbides and nitrides comprises e.g. functionalizing surface of magnetic filler with amino group, dispersing graphene in water, and emulsifying with an emulsification pump.
  • 专利号:   CN114854240-A, CN114854240-B
  • 发明人:   CHEN Z, YAN Q, WANG P, NING X, ZHANG M
  • 专利权人:   XINHUA ZHONGRUN CHEM TECHNOLOGY CO LTD
  • 国际专利分类:   C09D163/00, C09D005/08, C09D005/24, C09D005/32
  • 专利详细信息:   CN114854240-A 05 Aug 2022 C09D-005/24 202293 Chinese
  • 申请详细信息:   CN114854240-A CN10642920 08 Jun 2022
  • 优先权号:   CN10642920

▎ 摘  要

NOVELTY - Preparing conductive, wave-absorbing and anti-corrosion integrated coating based on two-dimentional carbides and nitrides (MXene) comprises e.g. (1) functionalizing surface of the magnetic filler with amino group, and obtain a magnetic material with amino groups on the surface, dispersing 1-10 pts. wt. graphene in 1-100 pts. wt. water, adding 1-5 pts. wt. non-ionic surfactant, adjusting pH to 9-11, then adding 1-100 pts. wt. magnetic material with amino groups on the surface, stirring at high speed for 10-30 minutes, then emulsifying with an emulsification pump for 30-60 minutes, and drying to obtain a mixture of graphene nanosheets-magnetic filler, and (2) adding 1-10 pts. wt. graphene, 1-10 pts. wt. Mxene, 1-100 pts. wt. magnetic filler with amino groups on surface to 1-100 pts. wt. water, adjusting pH to 9-11, then stirring at high speed for 1-60 minutes, performing emulsification treatment for 30-120 minutes with an emulsification pump. USE - The method is useful for preparing conductive, wave-absorbing and anti-corrosion integrated coating based on two-dimentional carbides and nitrides (MXene). ADVANTAGE - The coating: has good conductivity, wave-absorbing performance and anti-corrosion performance. DETAILED DESCRIPTION - Preparing conductive, wave-absorbing and anti-corrosion integrated coating based on two-dimentional carbides and nitrides (MXene) comprises (1) functionalizing surface of the magnetic filler with amino group, and obtain a magnetic material with amino groups on the surface, dispersing 1-10 pts. wt. graphene in 1-100 pts. wt. water, adding 1-5 pts. wt. non-ionic surfactant, adjusting pH to 9-11, then adding 1-100 pts. wt. magnetic material with amino groups on the surface, stirring at high speed for 10-30 minutes, then emulsifying with an emulsification pump for 30-60 minutes, and drying to obtain a mixture of graphene nanosheets-magnetic filler, (2) adding 1-10 pts. wt. graphene, 1-10 pts. wt. Mxene, 1-100 pts. wt. magnetic filler with amino groups on surface to 1-100 pts. wt. water, adjusting pH to 9-11, then stirring at high speed for 1-60 minutes, performing emulsification treatment for 30-120 minutes with an emulsification pump, and spray drying to form a composite filler of graphene nanosheets/Mxene/magnetic filler, (3) adding 1-50 pts. wt. graphene nanosheets-magnetic filler, 1-50 pts. wt. graphene nanosheets/Mxene/magnetic filler to 1-100 pts. wt. epoxy resin, adding 0.5-2 pts. wt. dispersing wetting agent, 0.5-1 pts. wt. anti-settling agent, 1-5 pts. wt. spherical conductive carbon black, 0.5-1 pts. wt. defoamer and 0.5-1 pts. wt. corrosion inhibitor to obtain finished coating.