• 专利标题:   Electrochemical deposition of graphene oxide on substrate during manufacture of electronic device, involves immersing electrode terminal including working electrode in graphene oxide solution, and depositing graphene oxide on electrode.
  • 专利号:   KR2015091447-A, KR1563261-B1
  • 发明人:   JEON M H, CHOI H K, CHOI Y S, GONG J S, PARK Y J, LIM Y J
  • 专利权人:   UNIV INJE IND ACADEMIC COOP FOUND
  • 国际专利分类:   B01J019/10, C01B031/04, C25D005/04, C25D005/50
  • 专利详细信息:   KR2015091447-A 11 Aug 2015 C25D-005/04 201562 Pages: 10
  • 申请详细信息:   KR2015091447-A KR101184 16 Jul 2015
  • 优先权号:   KR056828, KR101184

▎ 摘  要

NOVELTY - Electrochemical deposition of graphene oxide involves adding graphite to dispersion, oxidizing graphite solution, immersing electrode terminal including reference electrode, counter electrode, and working electrode as a substrate in obtained graphene oxide solution, depositing reduced graphene oxide on the working electrode by applying voltage of 2-5 V to the electrode terminal, and heat-treating the reduced graphene oxide deposited on the working electrode. USE - Electrochemical deposition of graphene oxide on substrate during manufacture of electronic device. ADVANTAGE - The method enables economical deposition of graphene oxide, in a short period of time, and improves electron transport property and electron transfer efficiency of the electronic device. DETAILED DESCRIPTION - Electrochemical deposition of graphene oxide involves adding graphite to dispersion, oxidizing graphite solution, immersing electrode terminal including reference electrode, counter electrode and working electrode as a substrate in obtained graphene oxide solution, depositing reduced graphene oxide on the working electrode by applying voltage of 2-5 V to the electrode terminal, and heat-treating the reduced graphene oxide deposited on the working electrode. The graphene oxide solution is prepared by chemical oxidation of graphite, mixing graphite oxide and polar solvent, and ultrasonically dispersing. The working electrode and the counter electrode are made of fluorine-doped tin oxide glass, such that the particle size of graphene oxide contained in the oxide solution is 10-500 nm.