• 专利标题:   Manufacture of graphene film for manufacture of patterned graphene film, involves dispersing grafted graphene obtained using graphite and benzene ring-containing monomer, in organic solvent, and spin-coating obtained solution on substrate.
  • 专利号:   KR2012023471-A, KR1321114-B1
  • 发明人:   BAE S Y, JEON I Y, BAEK J B
  • 专利权人:   UNIST ACADIND RES CORP
  • 国际专利分类:   B05D001/40, C01B031/02
  • 专利详细信息:   KR2012023471-A 13 Mar 2012 C01B-031/02 201310 Pages: 22
  • 申请详细信息:   KR2012023471-A KR086732 03 Sep 2010
  • 优先权号:   KR086732

▎ 摘  要

NOVELTY - Graphite and benzene ring-containing monomer having functional group(s) chosen from carboxylic acid group, amide group, sulfonic acid group, carbonylchloride and carbonyl bromide group, are reacted in reaction medium containing polyphosphate and phosphorus pentoxide, to obtain grafted graphene. Grafted graphene is dispersed in organic solvent, to obtain dispersion solution. Obtained dispersion solution is spin-coated on substrate. Resultant substrate is horizontally fitted, and processed, to obtain graphene film. USE - Manufacture of graphene film used for manufacture of patterned graphene film (all claimed). ADVANTAGE - The graphene film having high purity and quality, is manufactured, by simple method. The generation of graphite damage during manufacture of graphene film, is reduced. DETAILED DESCRIPTION - Graphite and organic compound having functional group(s) chosen from carboxylic acid group, amide group, sulfonic acid group, carbonylchloride and carbonyl bromide group are reacted in reaction medium containing polyphosphate and phosphorus pentoxide, to obtain organically functionalized graphene. Graphite and benzene ring-containing monomer having functional group(s) chosen from carboxylic acid group, amide group, sulfonic acid group, carbonylchloride and carbonyl bromide group, are reacted in reaction medium containing poly phosphate and phosphorus pentoxide, to obtain grafted graphene. Obtained organically functionalized graphene or grafted graphene is dispersed in organic solvent, to obtain dispersion solution (0.001-100 mg/ml). Obtained dispersion solution is dispersed or spin-coated on substrate. Resultant substrate is horizontally fitted, and processed for 0.01 second to 5 minutes, to obtain graphene film. An INDEPENDENT CLAIM is included for manufacture of patterned graphene film.