• 专利标题:   Manufacture of graphene oxide involves reacting graphite powder, concentrated sulfuric acid, potassium permanganate and hydrogen peroxide, filtering, washing, adding aqueous hydrochloride solution, drying, dialyzing, and centrifuging.
  • 专利号:   CN103382028-A
  • 发明人:   CHEN L, CHENG Z, GUO J, LIU Y, TAN S, WANG D, WANG M, YU S
  • 专利权人:   QINGDAO ZHONGKE HAOTAI NEW MATERIAL TECH
  • 国际专利分类:   C01B031/04, C02F009/04
  • 专利详细信息:   CN103382028-A 06 Nov 2013 C01B-031/04 201410 Pages: 8 Chinese
  • 申请详细信息:   CN103382028-A CN10232842 17 Aug 2013
  • 优先权号:   CN10232842

▎ 摘  要

NOVELTY - Manufacture of graphene oxide involves heating graphite powder and concentrated sulfuric acid at low temperature, adding potassium permanganate, reacting, adding water, reacting at high temperature, adding hydrogen peroxide solution, obtaining bright yellow solution, filtering, washing the filter cake, adding aqueous hydrochloride solution, drying the obtained solid, putting dried solid into water, stirring, dialyzing, and removing substrate by centrifuging. USE - Manufacture of graphene oxide (claimed). ADVANTAGE - The method enables efficient manufacture of stably dispersed solution of graphene oxide. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for method of processing of graphene oxide waste liquid, which involves diluting the filtrate obtained during manufacture of graphene oxide, adjusting pH to 10, aging, precipitating, separating clear liquid, and obtaining precipitate of manganese.